反应条件
1: 1.) NaH / 1.) THF, room temperature 45 min, reflux - 15 min, 2.) THF, 14 h
2: 80 percent / TFA / CH2Cl2 / 1.5 h / Ambient temperature
3: 60 percent / ceric ammonium nitrate
4: 98 percent / NH4Cl
View Scheme
参考文献
Roberts, David; Joule, John A.; Antonieta Bros; Alvarez, Mercedes
Journal of Organic Chemistry, 1997 , vol. 62, # 3 p. 568 - 577
