反应条件
1: PdCl2(CH3CN)2 / CH2Cl2 / 2 h / Ambient temperature 2: 1.) O3, 2.) Me2S / 1.) MeOH. -78 deg C, 2.) MeOH, RT, 5 h 3: NaBH4 / methanol / 3 h / Ambient temperature 4: LiAlH4 / tetrahydrofuran / 2 h / -50 °C 5: p-TsOH / acetone / 10 h / Ambient temperature View Scheme
参考文献
Saito, Seiki; Kuroda, Akiyoshi; Matsunaga, Hiroshi; Ikeda, Shushiro
Tetrahedron, 1996 , vol. 52, # 44 p. 13919 - 13932
