反应条件
1.1: 83 percent / Pd(PPh3)4P; aq. Na2CO3 / 1,2-dimethoxy-ethane / Heating
2.1: 88 percent / LDA / tetrahydrofuran / 6 h / 20 °C
3.1: LDA / tetrahydrofuran; hexane / 0.08 h / 0 °C
3.2: 65 percent / tetrahydrofuran; hexane / 0 - 20 °C
4.1: 73 percent / aq. HCO2H; Pd(OAc)2; Ph3P / dimethylformamide / 60 - 70 °C
View Scheme
参考文献
Fu, Jian-Min; Snieckus, Victor
Canadian Journal of Chemistry, 2000 , vol. 78, # 6 p. 905 - 919
