1-(2-氯-4-碘吡啶-3-基)乙酮合成路线 (共 3 条)
反应条件
pyridinium chlorochromate in dichloromethane 24 h; Ambient temperature;
参考文献
Guillier; Nivoliers; Cochennec; Godard; Marsais; Queguiner
Synthetic Communications, 1996 , vol. 26, # 23 p. 4421 - 4436
反应条件
lithium diisopropyl amide in tetrahydrofuran -70 deg C, 3 h, -10 deg C, 3 h;
参考文献
Guillier; Nivoliers; Cochennec; Godard; Marsais; Queguiner
Synthetic Communications, 1996 , vol. 26, # 23 p. 4421 - 4436
反应条件
1: 79 percent / LDA / tetrahydrofuran / 4.5 h / -70 °C 2: 98 percent / PCC / CH2Cl2 / 24 h / Ambient temperature View Scheme
参考文献
Guillier; Nivoliers; Cochennec; Godard; Marsais; Queguiner
Synthetic Communications, 1996 , vol. 26, # 23 p. 4421 - 4436