n-butyllithium in tetrahydrofuran; hexane 1.) -78 deg C to RT, overnight; 2.) -78 deg C to RT, 3 h;
参考文献
Seebach, Dieter; Amstutz, Rene; Laube, Thomas; Schweizer, W. Bernd; Dunitz, Jack D.
Journal of the American Chemical Society, 1985 , vol. 107, # 19 p. 5403 - 5409
1: in tetrahydrofuran 3 h; Inert atmosphere; 2: in hexane 0.25 h; Inert atmosphere;
参考文献
Kindra, Douglas R.; Casely, Ian J.; Fieser, Megan E.; Ziller, Joseph W.; Furche, Filipp; Evans, William J.
Journal of the American Chemical Society, 2013 , vol. 135, # 20 p. 7777 - 7787
