(3,3-二甲基环氧乙烷基)甲醇合成路线 （共 15 条）
反应条件
dihydrogen peroxide; {[CF3(CF2)7(CH2)3]3N(+)}12[WZn3(H2O)2(ZnW9O34)2] in ethyl acetate T=22°C; 8 h;
参考文献
Baumstark; Franklin; Vasquez; Crow
Molecules, 2004 , vol. 9, # 3 p. 117 - 124
反应条件
1: (1R,2R,4R)-2-exo-hydroperoxy-2-endo-(2'-furyl)-1,7,7-trimethylbicyclo[2.2.1]heptane With titanium(IV) isopropylate; MS 4 Angstroem in dichloromethane T=-20°C; 1 h; 2: 3,3-dimethylallyl alcohol in dichloromethane T=-20°C; 5 h;
参考文献
Lattanzi, Alessandra; Iannece, Patrizia; Vicinanza, Assunta; Scettri, Arrigo
Chemical Communications, 2003 , # 12 p. 1440 - 1441
反应条件
dihydrogen peroxide; dry-gel conversion Ti-Beta zeolite in water; acetonitrile T=49.85°C; Oxidation; 3 h;
参考文献
Tatsumi, Takashi; Jappar, Nizamidin
Journal of Physical Chemistry B, 1998 , vol. 102, # 37 p. 7126 - 7131
反应条件
dihydrogen peroxide; WO3; silica gel T=40°C; 2 h; Title compound not separated from byproducts;
参考文献
Somma, Filippo; Strukul, Giorgio
Journal of Catalysis, 2004 , vol. 227, # 2 p. 344 - 351
反应条件
dihydrogen peroxide; tetra-n-butyl-ammonium in acetonitrile T=31.85°C; 5 h;
参考文献
Kamata, Keigo; Kotani, Miyuki; Yamaguchi, Kazuya; Hikichi, Shiro; Mizuno, Noritaka
Chemistry - A European Journal, 2007 , vol. 13, # 2 p. 639 - 648
反应条件
titanium(IV) isopropylate; 4 A molecular sieve; 3-hydroperoxy-2,3-dimethyl-2-butanol in chloroform-d1 T=20°C; 1 h; Yield given;
参考文献
Adam, Waldemar; Peters, Karl; Renz, Michael
Journal of Organic Chemistry, 1997 , vol. 62, # 10 p. 3183 - 3189
反应条件
oxygen; isobutyraldehyde in acetonitrile T=34.84°C; 3 h;
参考文献
Zhang, Aiping; Li, Linqing; Li, Jun; Zhang, Yi; Gao, Shuang
Catalysis Communications, 2011 , vol. 12, # 13 p. 1183 - 1187
反应条件
sodium periodate 1.) CH2Cl2, heptane, room temp., 16 h, 2.) THF, H2O (1:1), room temp., 2 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Balasubramaniam, Rajiv P.; Moss, David K.; Wyatt, Justin K.; Spence, John D.; Gee, Arvin; Nantz, Michael H.
Tetrahedron, 1997 , vol. 53, # 22 p. 7429 - 7444
反应条件
in n-heptane; dichloromethane 16 h; Ambient temperature; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Balasubramaniam, Rajiv P.; Moss, David K.; Wyatt, Justin K.; Spence, John D.; Gee, Arvin; Nantz, Michael H.
Tetrahedron, 1997 , vol. 53, # 22 p. 7429 - 7444
反应条件
triethylamine in dichloromethane T=0°C; 1 h;
参考文献
Krief, Alain; Dumont, Willy; Baillieul, Diane
Synthesis, 2002 , # 14 p. 2019 - 2022
