4,4'-二氨基-2,2'-联吡啶合成路线 （共 7 条）
反应条件
hydrazine hydrate; palladium on activated charcoal in ethanol Reduction; 8 h; Heating;
参考文献
Maury; Guegana; Renouard; Hilton; Dupau; Sandon; Toupet; Le Bozec
New Journal of Chemistry, 2001 , vol. 25, # 12 p. 1553 - 1566
反应条件
ammonia in various solvent(s) T=160°C; 24 h;
参考文献
Araki, Koji; Mutai, Toshiki; Shigemitsu, Yasuhiro; Yamada, Masaki; Nakajima, Takayoshi; et al.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1996 , # 4 p. 613 - 618
反应条件
1: 86 percent / HNO3; H2SO4 / 20 h / 95 - 100 °C 2: hydrazine hydrate / Pd/C / ethanol / 15 h / Heating View Scheme
参考文献
Fabbrizzi, Pierangelo; Cecconi, Bianca; Cicchi, Stefano
Synlett, 2011 , # 2 art. no. G30910ST, p. 223 - 226
反应条件
1: With nitric acid 2: With 1 Pd/C
参考文献
Shang, Xue-Fang
Spectrochimica Acta - Part A: Molecular and Biomolecular Spectroscopy, 2009 , vol. 72, # 5 p. 1117 - 1121
反应条件
1: toluene-4-sulfonic acid / toluene / |Heating 2: NiBr2(PPh3)2; zinc; lithium chloride; tetraethylammonium iodide / tetrahydrofuran / |Heating 3: hydroxylamine hydrochloride; diethylamine / ethanol; water / |Heating View Scheme
参考文献
Kremer, Christopher; Schnakenburg, Gregor; Lutzen, Arne
Beilstein Journal of Organic Chemistry, 2014 , vol. 10, p. 814 - 824
反应条件
1: NiBr2(PPh3)2; zinc; lithium chloride; tetraethylammonium iodide / tetrahydrofuran / |Heating 2: hydroxylamine hydrochloride; diethylamine / ethanol; water / |Heating View Scheme
参考文献
Kremer, Christopher; Schnakenburg, Gregor; Lutzen, Arne
Beilstein Journal of Organic Chemistry, 2014 , vol. 10, p. 814 - 824
反应条件
in N,N-dimethyl-formamide
T=150 - 155°C; P=760.051 Torr; Inert atmosphere;
参考文献
BIO-NANO POWER; Long, Nathan R.; Wang, Jie; Abdelhady, Hosam Gharib
Patent: US2013/330293 A1, 2013 ;
Location in patent: Paragraph 0549; 0550 ;
