1,1,2-肼三羧酸三叔丁酯合成路线 （共 5 条）
反应条件
dihydroxy-(furan-2-yl)-borane; copper diacetate; 4 A molecular sieve in methanol T=40°C; 1 h;
参考文献
Kisseljova, Ksenija; Tsubrik, Olga; Sillard, Rannar; Maeeorg, Sirje; Maeeorg, Uno
Organic Letters, 2006 , vol. 8, # 1 p. 43 - 45
反应条件
hydrogen; palladium on activated charcoal in methanol 3 h; Yield given;
参考文献
Maeeorg, Uno; Grehn, Leif; Ragnarsson, Ulf
Angewandte Chemie, 1996 , vol. 108, # 22 p. 2802 - 2803
反应条件
1: 0.25 h 2: DMAP / acetonitrile / 0.25 h 3: H2 / 5percent Pd/C / methanol / 3 h View Scheme
参考文献
Maeeorg, Uno; Grehn, Leif; Ragnarsson, Ulf
Angewandte Chemie, 1996 , vol. 108, # 22 p. 2802 - 2803
反应条件
1: DMAP / acetonitrile / 0.25 h 2: H2 / 5percent Pd/C / methanol / 3 h View Scheme
参考文献
Maeeorg, Uno; Grehn, Leif; Ragnarsson, Ulf
Angewandte Chemie, 1996 , vol. 108, # 22 p. 2802 - 2803
反应条件
1: 100 percent / Cu(OAc)2; Et3N / CH2Cl2 / 23 h / 20 °C
2: 90 percent / Mg(ClO4)2 / acetonitrile / 0.83 h / 50 °C
View Scheme
参考文献
Loog; Maeorg; Ragnarsson
Synthesis, 2000 , # 11 p. 1591 - 1597
