3-乙炔苯基氨基甲酸叔丁酯合成路线 （共 4 条）
反应条件
in tetrahydrofuran Heating;
参考文献
Liu, Gang; Xin, Zhili; Pei, Zhonghua; Hajduk, Philip J.; Abad-Zapatero, Cele; Hutchins, Charles W.; Zhao, Hongyu; Lubben, Thomas H.; Ballaron, Stephen J.; Haasch, Deanna L.; Kaszubska, Wiweka; Rondinone, Cristina M.; Trevillyan, James M.; Jirousek, Michael R.
Journal of Medicinal Chemistry, 2003 , vol. 46, # 20 p. 4232 - 4235
反应条件
1: 77 percent / tetrahydrofuran / 120 h / Ambient temperature 2: 92 percent / Et3N, CuI, Pd(PPh3)2Cl2 / 2 h / 50 °C 3: 100 percent / K2CO3 / methanol / 1 h / Ambient temperature View Scheme
参考文献
Macdonald, Gregor; Lewis, Norman J.; Taylor, Richard J. K.
Chemical Communications, 1996 , # 23 p. 2647 - 2648
反应条件
1: 77 percent / tetrahydrofuran / 120 h / Ambient temperature 2: 92 percent / Et3N, CuI, Pd(PPh3)2Cl2 / 2 h / 50 °C 3: 100 percent / K2CO3 / methanol / 1 h / Ambient temperature View Scheme
参考文献
Macdonald, Gregor; Lewis, Norman J.; Taylor, Richard J. K.
Chemical Communications, 1996 , # 23 p. 2647 - 2648
反应条件
1: 92 percent / Et3N, CuI, Pd(PPh3)2Cl2 / 2 h / 50 °C 2: 100 percent / K2CO3 / methanol / 1 h / Ambient temperature View Scheme
参考文献
Macdonald, Gregor; Lewis, Norman J.; Taylor, Richard J. K.
Chemical Communications, 1996 , # 23 p. 2647 - 2648
