1-羟基-2-苯基-1H-吲哚合成路线 (共 30 条)
反应条件
α-[2-(2-butoxyethoxy)ethoxy]-4,5-methylenedioxy-2-propyltoluene; triethylammonium formate in methanol T=55°C; 12 h;
参考文献
Wong, Audrey; Kuethe, Jeffrey T.; Davies, Ian W.
Journal of Organic Chemistry, 2003 , vol. 68, # 25 p. 9865 - 9866
反应条件
1: 1.) TsCl, pyridine / 1.) DMF, -20 deg C, 30 min, 2.) DMF, -20 deg C, 4 h, RT, 1 d 2: 42.6 percent / Se / 5 h / 300 - 310 °C View Scheme
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 29, # 7 p. 1920 - 1926
反应条件
pyridine in N,N-dimethyl-formamide 3 h; Heating;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 29, # 7 p. 1920 - 1926
反应条件
acetic anhydride 3 h; Heating;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 29, # 7 p. 1920 - 1926
反应条件
acetic anhydride 3 h; Heating;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 29, # 7 p. 1920 - 1926
反应条件
in 1,4-dioxane Dimerization; reduction; oxidation; 6 h; Photolysis; Further byproducts given;
参考文献
Tetrahedron, , vol. 54, # 20 p. 5305 - 5314
反应条件
pyridine; p-toluenesulfonyl chloride 1.) DMF, -20 deg C, 30 min, 2.) DMF, -20 deg C, 4 h, RT, 3 d; Yield given. Multistep reaction;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 29, # 7 p. 1920 - 1926
反应条件
N-nitroso-diphenylamine; trichloroacetic acid in dichloromethane 1 h; Ambient temperature;
参考文献
Cardellini; Greci; Stipa
Synthetic Communications, 1994 , vol. 24, # 5 p. 677 - 682
反应条件
trichlorophosphate 0.75 h; Ambient temperature;
参考文献
Nagayoshi; Saeki; Hamana
Chemical and Pharmaceutical Bulletin, 1981 , vol. 29, # 7 p. 1827 - 1831
反应条件
in 1,2-dichloro-ethane 24 h; Ambient temperature; Yield given;
参考文献
Tosi, Giorgio; Cardellini, Liberato; Cardillo, Barbara; Bocelli, Gabrielle
Monatshefte fuer Chemie, 1987 , vol. 118, p. 369 - 380