1-羟基-2-苯基-1H-吲哚合成路线 (共 30 条)
反应条件
pyridine; p-toluenesulfonyl chloride
1.) DMF, -20 deg C, 30 min, 2.) DMF, -20 deg C, 4 h, RT, 1 d; Yield given. Multistep reaction;
参考文献
Nagayoshi, Tsuyoshi; Saeki, Seitaro; Hamana, Masatomo
Chemical and Pharmaceutical Bulletin, 1981 , vol. 29, # 7 p. 1920 - 1926
反应条件
pyridine in N,N-dimethyl-formamide
5 h; Heating;
参考文献
Nagayoshi, Tsuyoshi; Saeki, Seitaro; Hamana, Masatomo
Chemical and Pharmaceutical Bulletin, 1981 , vol. 29, # 7 p. 1920 - 1926
反应条件
acetic anhydride
3 h; Heating;
参考文献
Nagayoshi, Tsuyoshi; Saeki, Seitaro; Hamana, Masatomo
Chemical and Pharmaceutical Bulletin, 1981 , vol. 29, # 7 p. 1920 - 1926
反应条件
1-chlorobenzotriazole in dichloromethane
1 h; Ambient temperature;
参考文献
Berti, Corrado; Greci, Lucedio; Andruzzi, Romano; Trazza, Antonio
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1986 , p. 607 - 610
反应条件
acetic anhydride
3 h; Heating;
参考文献
Nagayoshi, Tsuyoshi; Saeki, Seitaro; Hamana, Masatomo
Chemical and Pharmaceutical Bulletin, 1981 , vol. 29, # 7 p. 1920 - 1926
反应条件
in 1,4-dioxane
Dimerization; reduction; oxidation; 6 h; Photolysis; Further byproducts given;
参考文献
Bruni, Paolo; Giorgini, Elisabetta; Tommasi, Giampaolo; Greci, Lucedio
Tetrahedron, 1998 , vol. 54, # 20 p. 5305 - 5314
反应条件
sodium carbonate in dichloromethane
120 h; Ambient temperature;
参考文献
Nagayoshi, Tsuyoshi; Saeki, Seitaro; Hamana, Masatomo
Chemical and Pharmaceutical Bulletin, 1981 , vol. 29, # 7 p. 1920 - 1926
反应条件
quinolinyl-N-oxide in chloroform
4 h; Heating;
参考文献
Nagayoshi; Saeki; Hamana
Chemical and Pharmaceutical Bulletin, 1981 , vol. 29, # 7 p. 1827 - 1831
反应条件
in chloroform
4 h; Heating;
参考文献
Nagayoshi; Saeki; Hamana
Chemical and Pharmaceutical Bulletin, 1981 , vol. 29, # 7 p. 1827 - 1831
反应条件
hydrogen iodide in water; acetonitrile
0.25 h; Ambient temperature;
参考文献
Berti, Corrado; Greci, Lucedio; Andruzzi, Romano; Trazza, Antonio
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1986 , p. 607 - 610