(1,4,5-三甲基-1H-咪唑-2-基)甲醇合成路线 （共 3 条）
反应条件
sodium tetrahydroborate in methanol 18 h; Ambient temperature;
参考文献
Alcalde, Ermitas; Alemany, Montserrat; Gisbert, Maria
Tetrahedron, 1996 , vol. 52, # 48 p. 15171 - 15188
反应条件
1: 1.) nBuLi / 1.) THF, hexane, -40 deg C, 1 h, 2.) THF, hexane, RT, 24 h 2: 78 percent / NaBH4 / methanol / 18 h / Ambient temperature View Scheme
参考文献
Tetrahedron, , vol. 52, # 48 p. 15171 - 15188
反应条件
1: 67 percent / thionyl chloride / CH2Cl2 / 5 h / Ambient temperature
2: 21 percent / dimethylformamide / 1 h / Ambient temperature
View Scheme
参考文献
Alcalde, Ermitas; Alemany, Montserrat; Gisbert, Maria
Tetrahedron, 1996 , vol. 52, # 48 p. 15171 - 15188
