2-(二甲基苯甲硅烷)-4,4,5,5-四甲基-1,3,2-二氧环戊硼烷合成路线 （共 71 条）
反应条件
in THF-d8 (tetrahydrofuran-d8) 0.0833333 h;
参考文献
European Journal of Inorganic Chemistry, , # 15 p. 2799 - 2806
反应条件
in THF-d8 (tetrahydrofuran-d8) 1 h;
参考文献
European Journal of Inorganic Chemistry, , # 15 p. 2799 - 2806
反应条件
in THF-d8 (tetrahydrofuran-d8) 1 h;
参考文献
European Journal of Inorganic Chemistry, , # 15 p. 2799 - 2806
反应条件
in THF-d8 (tetrahydrofuran-d8) 0.0833333 h;
参考文献
European Journal of Inorganic Chemistry, , # 15 p. 2799 - 2806
反应条件
1,3-bis-(diphenylphosphino)propane; triethylamine; [(1,3-bis(Ph2P)propane)Rh(1,5-cyclooctadiene)]ClO4 in 1,4-dioxane; water T=50°C; 16 h;
参考文献
Walter, Christian; Froehlich, Roland; Oestreich, Martin
Tetrahedron, 2009 , vol. 65, # 28 p. 5513 - 5520
反应条件
1: Me2PhSiBpin With potassium methanolate in ethylene glycol dimethyl ether T=0°C; 0.166667 h; Inert atmosphere; 2: 1-bromo-4-methoxy-benzene in ethylene glycol dimethyl ether T=0°C; 1 h; SolventReagent/catalystTemperature; Overall yield = 83 percentChromat.;
参考文献
Yamamoto, Eiji; Izumi, Kiyotaka; Horita, Yuko; Ito, Hajime
Journal of the American Chemical Society, 2012 , vol. 134, # 49 p. 19997 - 20000
反应条件
1: Me2PhSiBpin With potassium methanolate in ethylene glycol dimethyl ether T=30°C; 0.166667 h; Inert atmosphere; 2: 1-methoxy-4-chlorobenzene in ethylene glycol dimethyl ether T=30°C; 1 h; Overall yield = 27 percentChromat.;
参考文献
Yamamoto, Eiji; Izumi, Kiyotaka; Horita, Yuko; Ito, Hajime
Journal of the American Chemical Society, 2012 , vol. 134, # 49 p. 19997 - 20000
反应条件
1: Me2PhSiBpin With potassium methanolate in ethylene glycol dimethyl ether T=30°C; 0.166667 h; Inert atmosphere; 2: 1-bromo-4-methoxy-benzene in ethylene glycol dimethyl ether T=30°C; 1 h; SolventTemperature;
参考文献
Yamamoto, Eiji; Izumi, Kiyotaka; Horita, Yuko; Ito, Hajime
Journal of the American Chemical Society, 2012 , vol. 134, # 49 p. 19997 - 20000
反应条件
1: Me2PhSiBpin With potassium methanolate in ethylene glycol dimethyl ether T=30°C; 0.166667 h; Inert atmosphere; 2: para-iodoanisole in ethylene glycol dimethyl ether T=30°C; 1 h;
参考文献
Yamamoto, Eiji; Izumi, Kiyotaka; Horita, Yuko; Ito, Hajime
Journal of the American Chemical Society, 2012 , vol. 134, # 49 p. 19997 - 20000
反应条件
1: Me2PhSiBpin With potassium methanolate in ethylene glycol dimethyl ether T=0°C; 0.166667 h; Inert atmosphere; 2: 1-bromo-4-methoxy-benzene in ethylene glycol dimethyl ether T=0°C; 1 h; SolventReagent/catalystTemperature; Overall yield = 83 percentChromat.;
参考文献
Yamamoto, Eiji; Izumi, Kiyotaka; Horita, Yuko; Ito, Hajime
Journal of the American Chemical Society, 2012 , vol. 134, # 49 p. 19997 - 20000
