(S)-2,2-二甲基-1,3-二氧戊环-4-乙酰胺合成路线 (共 3 条)
反应条件
1: With sulfuric acid in acetone T=20 - 60°C; 12.5 h; 2: With silver(l) oxide in acetone 1 h; Product distribution / selectivity;
参考文献
Michigan State University
Patent: EP1086072 B1, 2006 ;
Location in patent: Page/Page column 7; 8-9 ;
反应条件
ammonia in water 24 h; Ambient temperature;
参考文献
Critcher, Douglas J.; Pattenden, Gerald
Tetrahedron Letters, 1996 , vol. 37, # 50 p. 9107 - 9110
反应条件
sodium hydroxide; sodium hypochlorite in water
T=50 - 60°C; Hoffman reaction; 24 h;
参考文献
Wang, Guijun; Hollingsworth, Rawle I.
Journal of Organic Chemistry, 1999 , vol. 64, # 3 p. 1036 - 1038