3-[2-(2-(2-羟基乙氧基)乙氧基)乙氧基]丙酸叔丁酯 三乙二醇-O-丙酸叔丁酯合成路线 （共 2 条）
反应条件
1: 1,2-bis-(2-hydroxyethoxy)-ethane With sodium in tetrahydrofuran T=20°C; 2: 2-Propenoic acid tert-butyl ester in tetrahydrofuran T=20°C; 20 h; 3: With hydrogenchloride; water in tetrahydrofuran
参考文献
Wilbur, D. Scott; Pathare, Pradip M.; Hamlin, Donald K.; Wan, Feng
Patent: US2006/228325 A1, 2006 ;
Location in patent: Page/Page column 63 ;
反应条件
sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate in dichloromethane; water 0.75 h;
参考文献
Seitz, Oliver; Kunz, Horst
Journal of Organic Chemistry, 1997 , vol. 62, # 4 p. 813 - 826
