4-甲氧基-N,N-二苄基苯胺合成路线 (共 19 条)
反应条件
diethyl-1,4-dihydro-2,6-dimethyl-3,5-pyridine dicarboxylate in neat (no solvent) T=150°C; 12 h; Molecular sieve; TemperatureTime;
参考文献
Nguyen, Quynh Pham Bao; Kim, Taek Hyeon
Tetrahedron, 2013 , vol. 69, # 24 p. 4938 - 4943
反应条件
tetrabutylammomium bromide; sodium hydroxide in water T=70 - 100°C; 5.5 h;
参考文献
Shamim, Tahira; Kumar, Vineet; Paul, Satya
Synthetic Communications, 2014 , vol. 44, # 5 p. 620 - 632
反应条件
1: para-iodoanisole With iso-propylmagnesium bromide in tetrahydrofuran T=20°C; 1 h; 2: With zinc(II) chloride in tetrahydrofuran T=20°C; 0.166667 h; 3: Bn2N-OBz With copper (I) trifluoromethane sulfonate benzene in tetrahydrofuran T=25°C; 1 h;
参考文献
Nguyen, Minh H.; Smith, Amos B.
Organic Letters, 2013 , vol. 15, # 18 p. 4872 - 4875
反应条件
W4 Raney nickel in anhydrous xylene 32 h; Reflux;
参考文献
Mehta, Astha; Thaker; Londhe; Nandan, Santosh R.
Applied Catalysis A: General, 2014 , vol. 478, p. 241 - 251
反应条件
Au/Fe2O3 T=160°C; 8 h; Inert atmosphere; chemoselective reaction;
参考文献
Peng, Qiling; Zhang, Yan; Shi, Feng; Deng, Youquan
Chemical Communications, 2011 , vol. 47, # 22 p. 6476 - 6478
反应条件
1: tris(4-methoxyphenyl)boronic acid anhydride With potassium carbonate in 1,4-dioxane T=130°C; 24 h; Inert atmosphere; 2: Bn2N-OBz in 1,4-dioxane Inert atmosphere;
参考文献
Xiao, Qing; Tian, Leiming; Tan, Renchang; Xia, Ying; Qiu, Di; Zhang, Yan; Wang, Jianbo
Organic Letters, 2012 , vol. 14, # 16 p. 4230 - 4233
反应条件
copper(l) iodide; biphenyl-2-yl-di-tert-butyl-phosphane; lithium tert-butylate in 1,4-dioxane T=20°C; 4 h; Inert atmosphereSchlenk technique;
参考文献
Miki, Yuya; Hirano, Koji; Satoh, Tetsuya; Miura, Masahiro
Organic Letters, 2013 , vol. 15, # 1 p. 172 - 175
反应条件
phosphonitrilic chloride trimer in 1,2,4-trimethyl benzene T=160°C; 15 h; Inert atmosphere;
参考文献
Du, Ya; Oishi, Shunsuke; Saito, Susumu
Chemistry - A European Journal, 2011 , vol. 17, # 44 p. 12262 - 12267
反应条件
NSC26899 in acetonitrile T=20°C; Addition; benzylation; 2.5 h; Irradiation;
参考文献
Jin; Zhang; Yang; Liu
Tetrahedron Letters, 2000 , vol. 41, # 38 p. 7357 - 7360
反应条件
bis(1,2-diphenylphosphino)benzene; copper (II) acetate monohydrate; lithium tert-butylate in tetrahydrofuran T=20°C; Chan-Lam type coupling; 4 h; Inert atmosphere;
参考文献
Matsuda, Naoki; Hirano, Koji; Satoh, Tetsuya; Miura, Masahiro
Angewandte Chemie - International Edition, 2012 , vol. 51, # 15 p. 3642 - 3645