4-甲氧基-N,N-二苄基苯胺合成路线 （共 19 条）
反应条件
di-tert-butyl peroxide; copper diacetate in toluene T=50°C; 24 h; Sealed tubeInert atmosphere;
参考文献
Sueki, Shunsuke; Kuninobu, Yoichiro
Organic Letters, 2013 , vol. 15, # 7 p. 1544 - 1547
反应条件
1: 4-MeOC6H4Li With 3-butyl-1,1-diethyl-1,3-dihydrobenzo[c][1,2]oxasilole in tetrahydrofuran T=-78 - 20°C; 3 h; Inert atmosphere; 2: Bn2N-OBz With copper(l) iodide; dpca in tetrahydrofuran T=20°C; 2 h; Inert atmosphere;
参考文献
THE TRUSTEES OF THE UNIVERSITY OF PENNSYLVANIA; HOYE, Adam, T.; KIM, Won-suk; MARTINEZ-SOLORIO, Dionicio; SMITH, Amos, B.; SANCHEZ, Luis; TONG, Rongbiao; NGUYEN, Minh, Huu
Patent: WO2013/185021 A2, 2013 ;
Location in patent: Paragraph 0064 ;
反应条件
sodium t-butanolate; [P(o-tolyl)3]2; palladium dichloride in toluene 0.1 h; Irradiationmicrowave;
参考文献
Sharifi, Ali; Hosseinzadeh, Rahman; Mirzaei, Mojtaba
Monatshefte fur Chemie, 2002 , vol. 133, # 3 p. 329 - 332
反应条件
copper(l) iodide; N,N-dimethylaminoacetic acid; potassium carbonate in dimethyl sulfoxide T=110°C; 40 h;
参考文献
Zhang, Hui; Cai, Qian; Ma, Dawei
Journal of Organic Chemistry, 2005 , vol. 70, # 13 p. 5164 - 5173
反应条件
silica gel T=20°C; 12 h;
参考文献
Basu, Basudeb; Paul, Susmita; Nanda, Ashis K.
Green Chemistry, 2009 , vol. 11, # 8 p. 1115 - 1120
反应条件
1.1: dipotassium hydrogenphosphate trihydrate / N,N-dimethyl-formamide / 20 °C / Inert atmosphere 2.1: potassium carbonate / 1,4-dioxane / 24 h / 130 °C / Inert atmosphere 2.2: Inert atmosphere View Scheme
参考文献
Herman, Ashley M.; Johnson, Jeffrey S.
Journal of Organic Chemistry, 2006 , vol. 71, # 1 p. 219 - 224
反应条件
1: Inert atmosphere 2: bis(1,2-diphenylphosphino)benzene; copper (II) acetate monohydrate; lithium tert-butylate / tetrahydrofuran / 4 h / 20 °C / Inert atmosphere View Scheme
参考文献
Matsuda, Naoki; Hirano, Koji; Satoh, Tetsuya; Miura, Masahiro
Angewandte Chemie - International Edition, 2012 , vol. 51, # 15 p. 3642 - 3645
反应条件
[Pd(N,N′-bis(2,6-bis(diphenylmethyl)-4-methoxyphenyl)imidazol-2-ylidene)(acac)Cl]; potassium tert-butylate in 1,4-dioxane T=20°C; Buchwald-Hartwig Coupling; 18 h; Inert atmosphereGlovebox; Catalytic behavior; Reagent/catalyst;
参考文献
Meiries, Sebastien; Speck, Klaus; Cordes, David B.; Slawin, Alexandra M. Z.; Nolan, Steven P.
Organometallics, 2013 , vol. 32, # 1 p. 330 - 339
反应条件
tris(triphenylphosphine)ruthenium(II) chloride T=150°C; Product distributionRate constantMechanism;
参考文献
Watanabe, Yoshihisa; Tsuji, Yasushi; Ige, Hitoshi; Ohsugi, Yukihiro; Ohta, Tetsuo
Journal of Organic Chemistry, 1984 , vol. 49, # 18 p. 3359 - 3363
