1-(5-氯-2-硝基)苯乙酮合成路线 （共 9 条）
反应条件
sulfuric acid; nitric acid T=-20 - -10°C; 5.25 h;
参考文献
US2007/238700 A1, ;
Page/Page column 26 ;
反应条件
sulfuric acid; nitric acid in water T=-5°C; 3 h;
参考文献
US2012/15908 A1, ;
Page/Page column 24 ;
反应条件
hydrogenchloride; copper(l) chloride T=5 - 10°C;
参考文献
Journal of the Chemical Society, , p. 646,655
反应条件
1: sulfuric acid; nitric acid 2: aqueous hydrochloric acid 3: aqueous HCl; CuCl / 5 - 10 °C View Scheme
参考文献
Journal of the Chemical Society, , p. 646,655
反应条件
1: aqueous hydrochloric acid 2: aqueous HCl; CuCl / 5 - 10 °C View Scheme
参考文献
Journal of the Chemical Society, , p. 646,655
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 17, p. 596 - 604
反应条件
1: 93.3 percent / dimethylformamide / 4.5 h / 110 °C 2: 77 percent / FeSO4*7H2O / ethanol; H2O / 0.17 h / Heating View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 30, # 8 p. 1421 - 1426
反应条件
hydrogen; platinum(IV) oxide in ethanol T=20°C; P=760.051 Torr; 4.5 h;
参考文献
Meyer, Adam Gerhard; Winzenberg, Kevin Norman; Sawutz, David G.; Liepa, Andris Juris
Patent: US2006/63841 A1, 2006 ;
Location in patent: Page/Page column 24; 4/12 ;
反应条件
1: H2 / 10percent Pd/C
View Scheme
参考文献
Li, Leping; Wang, Hui-Kang; Kuo, Sheng-Chu; Wu, Tian-Shung; Mauger, Anthony; et al.
Journal of Medicinal Chemistry, 1994 , vol. 37, # 20 p. 3400 - 3407
