4-氨基呋喃并[2,3-D]嘧啶合成路线 (共 3 条)
参考文献
WO2007/38387 A2, ;
Page/Page column 80-81 ;
反应条件
chloro-trimethyl-silane; tert.-butylnitrite in acetonitrile T=50°C; Sandmeyer reaction; 1.5 h;
参考文献
YALE UNIVERSITY
Patent: WO2007/38387 A2, 2007 ;
Location in patent: Page/Page column 80-81 ;
反应条件
1: 40 percent / tert-butyl nitrite; TMSCl / acetonitrile / 1.5 h / 50 °C
2: HCl / ethanol; H2O / 90 °C
View Scheme
参考文献
Kim, Joseph T.; Hamilton, Andrew D.; Bailey, Christopher M.; Domoal, Robert A.; Wang, Ligong; Anderson, Karen S.; Jorgensen, William L.
Journal of the American Chemical Society, 2006 , vol. 128, # 48 p. 15372 - 15373