3,5,6-三甲基-哌嗪-2-甲醛合成路线 （共 4 条）
反应条件
phosphoric acid; dicyclohexyl-carbodiimide in dimethyl sulfoxide Pfitzner-Moffatt oxidation;
参考文献
Deng, Lijuan; Guo, Xiuli; Zhai, Li; Song, Yuning; Chen, Hongfei; Zhan, Peng; Wu, Jingde; Liu, Xinyong
Chemical Biology and Drug Design, 2012 , vol. 79, # 5 p. 731 - 739
反应条件
1: dihydrogen peroxide; acetic acid / 95 °C 2: 2 h / Reflux 3: sodium hydroxide 4: phosphoric acid; dicyclohexyl-carbodiimide / dimethyl sulfoxide View Scheme
参考文献
Chemical Biology and Drug Design, , vol. 79, # 5 p. 731 - 739
反应条件
1: 2 h / Reflux 2: sodium hydroxide 3: phosphoric acid; dicyclohexyl-carbodiimide / dimethyl sulfoxide View Scheme
参考文献
Chemical Biology and Drug Design, , vol. 79, # 5 p. 731 - 739
反应条件
sodium chlorite; 2-methyl-but-2-ene in water; tert-butyl alcohol T=0 - 20°C; 0.833333 h;
参考文献
MITSUBISHI TANABE PHARMA CORPORATION; KAWANISHI, Eiji; HONGU, Mitsuya; TANAKA, Yoshihito
Patent: WO2011/105628 A1, 2011 ;
Location in patent: Page/Page column 78 ;
WO 2011/105628 A1
