3-(2-氯苯基)-1-丙胺合成路线 (共 8 条)
反应条件
lithium aluminium tetrahydride in diethyl ether 4 h; Heating;
参考文献
Kerr, David I. B.; Ong, Jennifer; Perkins, Michael V.; Prager, Rolf H.; Puspawati, Ni Made
Australian Journal of Chemistry, 2006 , vol. 59, # 7 p. 445 - 456
反应条件
lithium aluminium tetrahydride in diethyl ether Reduction; 0.5 h;
参考文献
Hansen, Marcus C.; Buchwald, Stephen L.
Tetrahedron Letters, 1999 , vol. 40, # 11 p. 2033 - 2034
反应条件
chlorine in tetradeuterioacetic acid T=25°C; Product distributionKinetics; Further Variations:Solvents;
参考文献
Organic and Biomolecular Chemistry, , vol. 4, # 14 p. 2716 - 2723
反应条件
aluminium trichloride 12 h; Heating2 equivalents of AlCl3; Yield given. Title compound not separated from byproducts;
参考文献
Tetrahedron Letters, , vol. 21, p. 1719 - 1722
参考文献
Chemische Berichte, , vol. 56, p. 1483
反应条件
titanium(IV) isopropylate T=20°C;
参考文献
Kerr, David I. B.; Ong, Jennifer; Perkins, Michael V.; Prager, Rolf H.; Puspawati, Ni Made
Australian Journal of Chemistry, 2006 , vol. 59, # 7 p. 445 - 456
反应条件
bis(acetylacetonate)nickel(II); sodium t-butanolate; IPr*hydrochloride in 1,4-dioxane T=100°C; 4 h;
参考文献
Omar-Amrani, Rafik; Thomas, Antoine; Brenner, Eric; Schneider, Raphael; Fort, Yves
Organic Letters, 2003 , vol. 5, # 13 p. 2311 - 2314
反应条件
1: N,N'-bis(2,6-diisopropylphenyl)dihydroimidazol-2-ylidene*HCl; NaH; t-BuOH / Pd(OAc)2 / dioxane / 3 h 2: dioxane / 5 h View Scheme
参考文献
Omar-Amrani, Rafik; Schneider, Raphael; Fort, Yves
Synthesis, 2004 , # 15 p. 2527 - 2534