二-1H-茚-1-基-二甲基硅烷合成路线 (共 4 条)
反应条件
magnesium in tetrahydrofuran; ethylene dibromide Cooling with ice;
参考文献
Idemitsu Kosan Co., Ltd.; YABUGAMI, Minoru; OKAMOTO, Takuji
Patent: EP2650300 A1, 2013 ;
Location in patent: Paragraph 0045; 0046 ;
反应条件
1: CH2-indene With n-butyllithium in diethyl ether; hexane T=-78 - 20°C; 2: dimethyl-dichlorosilane in hexane T=-78 - 20°C;
参考文献
Journal of Organometallic Chemistry, , vol. 664, # 1-2 p. 5 - 26
反应条件
1: CH2-indene With n-butyllithium 2: dimethyl-dichlorosilane
参考文献
European Journal of Inorganic Chemistry, , # 5 p. 972 - 979
参考文献
Sommer, L. H.; Marans, N. S.
Journal of the American Chemical Society, 1951 , vol. 73, p. 5135 - 5138