2,2'-azo-bisisobutyronitrile; tri-n-butyl-tin hydride in benzene
3 h; Inert atmosphereReflux;
参考文献
Larraufie, Marie-Helene; Courillon, Christine; Ollivier, Cyril; Lacote, Emmanuel; Malacria, Max; Fensterbank, Louis
Journal of the American Chemical Society, 2010 , vol. 132, # 12 p. 4381 - 4387
phenanthrene in acetonitrile
43 h; Irradiationother electron-deficient alkenes; other asymmetrically substituted disilanes; relative quantum yields, effect of solvents on the photosilylation; Product distributionMechanism;
1: malononitrile With sodium in toluene
T=70°C; 2 h;
2: 5-benzylidene-2-morpholino-1,3-thiazol-4(5H)-one in toluene
T=70°C; 72 h; Title compound not separated from byproducts;
参考文献
Kandeel, Kamal A.; Youssef, Ali M.; EI-Bestawy, Hany M.; Omar, Mohamed T.
Monatshefte fur Chemie, 2002 , vol. 133, # 9 p. 1211 - 1219
Diez-Barra, Enrique; Hoz, Antonio de la; Moreno, Andres; Sanchez-Verdu, Prado
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1991 , # 4 p. 2589 - 2592