trichlorophosphate Heating;

1: anschliessend mit NH3 in Benzol 2: aq. NaOH solution 3: N,N-dimethyl-aniline; POCl3 View Scheme

1: aq. NaOH solution 2: N,N-dimethyl-aniline; POCl3 View Scheme

1: hydrogenchloride; trifluoroacetic acid; sodium nitrite / water / 1 h / 20 °C 2: trichlorophosphate / 3 h / Reflux View Scheme

1.1: hydrogenchloride / water / Reflux 2.1: diethyl ether / 1 h / 100 °C 2.2: 3 h / 50 - 110 °C 2.3: 3 h / 50 - 110 °C 3.1: hydrogenchloride; trifluoroacetic acid; sodium nitrite / water / 1 h / 20 °C 4.1: trichlorophosphate / 3 h / Reflux View Scheme

1.1: triethylamine / dichloromethane 2.1: nitric acid; acetic anhydride / dichloromethane 3.1: hydrogenchloride / water / Reflux 4.1: diethyl ether / 1 h / 100 °C 4.2: 3 h / 50 - 110 °C 4.3: 3 h / 50 - 110 °C 5.1: hydrogenchloride; trifluoroacetic acid; sodium nitrite / water / 1 h / 20 °C 6.1: trichlorophosphate / 3 h / Reflux View Scheme

1.1: nitric acid; acetic anhydride / dichloromethane 2.1: hydrogenchloride / water / Reflux 3.1: diethyl ether / 1 h / 100 °C 3.2: 3 h / 50 - 110 °C 3.3: 3 h / 50 - 110 °C 4.1: hydrogenchloride; trifluoroacetic acid; sodium nitrite / water / 1 h / 20 °C 5.1: trichlorophosphate / 3 h / Reflux View Scheme

暂无反应条件数据

in ethanol T=20°C;

ammonium chloride; zinc in water; acetic acid