1-(-2-氯-乙烯基)-4-甲氧基苯合成路线 (共 14 条)
反应条件
anhydrous lithium acetate; 1-chlorobenzotriazole in acetonitrile
T=50°C; 0.0833333 h; microwave irradiation;
参考文献
Katritzky, Alan R.; Majumder, Suman; Jain, Ritu
Journal of the Indian Chemical Society, 2003 , vol. 80, # 11 p. 1073 - 1075
反应条件
N-chloro-succinimide; iodosylbenzene in water; acetonitrile
T=60°C; 0.5 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Graven, Anette; Joergensen, Karl Anker; Dahl, Soeren; Stanczak, Andrzej
Journal of Organic Chemistry, 1994 , vol. 59, # 13 p. 3543 - 3546
反应条件
in cyclohexane
T=10°C; Irradiation;
参考文献
Tomioka, Hideo; Hayashi, Norihiro; Izawa, Yasuji; Liu, Michael T. H.
Journal of the Chemical Society, Chemical Communications, 1984 , # 7 p. 476 - 478
反应条件
in various solvent(s)
T=10°C; Irradiation; Yield given. Yields of byproduct given;
参考文献
Tomioka, Hideo; Hayashi, Norihiro; Izawa, Yasuji; Liu, Michael T. H.
Journal of the American Chemical Society, 1984 , vol. 106, # 2 p. 454 - 456
反应条件
chlorine dioxide in tetrachloromethane
T=52 - 54°C; 1.16667 h; Further byproducts given. Title compound not separated from byproducts;
参考文献
Kwiecien, Halina; Jalowiczor, Jozef
Polish Journal of Chemistry, 1986 , vol. 60, # 7-12 p. 811 - 824
反应条件
chlorine dioxide in tetrachloromethane
T=52 - 54°C; 1.16667 h; Further byproducts given;
参考文献
Kwiecien, Halina; Jalowiczor, Jozef
Polish Journal of Chemistry, 1986 , vol. 60, # 7-12 p. 811 - 824
反应条件
[Me4N][BF4] in N,N-dimethyl-formamide
Ambient temperaturecontrolled potential electrolysis; cathode: Hg; electrode ref.: AgI/Ag; Yield given. Further byproducts given. Yields of byproduct given;
参考文献
Le Menn, Jean-Christophe; Sarrazin, Jean; Tallec, Andre
Canadian Journal of Chemistry, 1989 , vol. 67, p. 1332 - 1343
反应条件
ammonium cerium (IV) nitrate; lithium chloride
T=20°C; 4 h; Mechanical activation;
参考文献
Nikishin; Sokova; Makhaev; Kapustina
Russian Chemical Bulletin, 2008 , vol. 57, # 1 p. 118 - 123
反应条件
in cyclohexane
T=10°C; Irradiation;
参考文献
Tomioka, Hideo; Hayashi, Norihiro; Izawa, Yasuji; Liu, Michael T. H.
Journal of the Chemical Society, Chemical Communications, 1984 , # 7 p. 476 - 478
反应条件
lithium diisopropyl amide in tetrahydrofuran; hexane
-78 deg C, 3 h then rt., 1 h; Yield given. Yields of byproduct given;
参考文献
Baudin, J. B.; Hareau, G.; Julia, S. A.; Lorne, R.; Ruel, O.
Bulletin de la Societe Chimique de France, 1993 , vol. 130, p. 856 - 878