3-溴-7,12-二苯基苯并[k]荧蒽合成路线 （共 5 条）
反应条件
1: in toluene 16 h; Reflux; 2: With hydrogen bromide; acetic acid in water T=80°C;
参考文献
Idemitsu Kosan Co., Ltd.; ITO, Hirokatsu; KAWAMURA, Masahiro; KAWAMURA, Yuichiro; MIZUKI, Yumiko; SAITO, Hiroyuki
Patent: EP2597094 A1, 2013 ;
Location in patent: Paragraph 0084 ;
反应条件
N-bromosuccinmide in 1-methyl-pyrrolidin-2-one; dichloromethane T=20°C; 20 h;
参考文献
BASF SE; BASF (CHINA) COMPANY LIMITED; KOeNEMANN, Martin; MATTERN, Gabriele; HWANG, Jae, Hyung; HOeH, Regina; DOeRR, Christian; TANABE, Junichi
Patent: WO2012/123888 A1, 2012 ;
Location in patent: Page/Page column 60-61 ;
反应条件
isopentyl nitrite in toluene T=110°C; 5 h; Inert atmosphere;
参考文献
CANON KABUSHIKI KAISHA; Nishide, Yosuke; Yamada, Naoki; Saitoh, Akihito
Patent: US2013/50561 A1, 2013 ;
Location in patent: Paragraph 0134; 0137-0139 ;
反应条件
1.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / benzene / 6 h / Reflux 2.1: toluene / 16 h / Reflux 2.2: 1 h / 80 °C View Scheme
参考文献
Idemitsu Kosan Co., Ltd.
Patent: EP2495240 A1, 2012 ;
反应条件
1: potassium hydroxide / ethanol / 3 h / 70 °C 2: isopentyl nitrite / toluene / 5 h / 110 °C / |Inert atmosphere View Scheme
参考文献
CANON KABUSHIKI KAISHA; Nishide, Yosuke; Yamada, Naoki; Saitoh, Akihito
Patent: US2013/50561 A1, 2013 ;
