3-乙氧基-1,2-苯并噻唑1,1-二氧化物合成路线 （共 20 条）
参考文献
Chemische Berichte, , vol. 26, p. 2292
反应条件
in tetrahydrofuran 1) -78 deg C, 4 h, 2) 25 deg C, 3 h;
参考文献
Davis; Towson; Vashi; ThimmaReddy; McCauley Jr.; Harakal; Gosciniak
Journal of Organic Chemistry, 1990 , vol. 55, # 4 p. 1254 - 1261
反应条件
1: aq. H2O2, K2CO3, p-tolyl methyl sulfide / methanol 2: 45 percent / tetrahydrofuran / 5 h / -78 °C View Scheme
参考文献
Page, Philip C. Bulman; Bethell, Donald; Stocks, Paul A.; Heer, Jag P.; Graham, Andrew E.; et al.
Synlett, 1997 , # 12 p. 1355 - 1358
反应条件
1: aq. H2O2, K2CO3, p-tolyl methyl sulfide / methanol
2: 40 percent / tetrahydrofuran / 5 h / -78 °C
View Scheme
参考文献
Page, Philip C. Bulman; Bethell, Donald; Stocks, Paul A.; Heer, Jag P.; Graham, Andrew E.; et al.
Synlett, 1997 , # 12 p. 1355 - 1358
反应条件
in acetonitrile
T=180°C; 20 h;
参考文献
Abramovitch, Rudolph A.; Shinkai, Ichiro; Mavunkel; More; O'Connor, Sean; Ooi, Gino H.; Pennington, William T.; Srinivasan; Stowers, James R.
Tetrahedron, 1996 , vol. 52, # 9 p. 3339 - 3354
反应条件
1: 90 percent / acetonitrile / 20 h / 180 °C
2: 70 percent / H2SO4 / 20 h / Heating
View Scheme
参考文献
Abramovitch,R.A. et al.
Heterocycles, 1976 , vol. 5, p. 95 - 99
反应条件
1: acetonitrile
2: aq. H2SO4
3: N2H4
View Scheme
参考文献
Abramovitch,R.A. et al.
Heterocycles, 1976 , vol. 5, p. 95 - 99
反应条件
1: bromobenzene With n-butyllithium in tetrahydrofuran
T=-78°C; Inert atmosphere;
2: O-ethyl saccharin in tetrahydrofuran
T=-78 - 20°C; 3 h; Inert atmosphere;
参考文献
Rommel, Michael; Fukuzumi, Takeo; Bode, Jeffrey W.
Journal of the American Chemical Society, 2008 , vol. 130, p. 17266 - 17267
反应条件
in tetrahydrofuran
T=-78°C; 4 h;
参考文献
Davis; Towson; Vashi; ThimmaReddy; McCauley Jr.; Harakal; Gosciniak
Journal of Organic Chemistry, 1990 , vol. 55, # 4 p. 1254 - 1261
反应条件
1: aq. H2O2, K2CO3, p-tolyl methyl sulfide / methanol
2: 53 percent / tetrahydrofuran / 5 h / -78 °C
View Scheme
参考文献
Page, Philip C. Bulman; Bethell, Donald; Stocks, Paul A.; Heer, Jag P.; Graham, Andrew E.; et al.
Synlett, 1997 , # 12 p. 1355 - 1358
