反应条件
1: 77 percent / NaN3 / dimethylformamide 2: 5percent HCl 3: SOCl2, Et3N / CH2Cl2 / 0.17 h / 0 °C 4: NaIO4, RuCl3 / CCl4; acetonitrile; H2O / 1 h / 20 °C 5: 78 percent / hydrogen / 10percent Pd/C / H2O; tetrahydrofuran / 2 h / 1551.4 Torr 6: H2SO4, H2O / tetrahydrofuran / 1 h / 90 °C 7: CH2Cl2 / 1 h / 25 °C 8: 84 percent / (COCl)2, DMSO, Et3N / 0.5 h / -70 - 25 °C View Scheme
参考文献
Albertini, Enrichetta; Barco, Achille; Benetti, Simonetta; De Risi, Carmela; Pollini, Gian P.; Zanirato, Vinicio
Tetrahedron Letters, 1997 , vol. 38, # 4 p. 681 - 684
