1: With potassium hexamethylsilazane in tetrahydrofuran; toluene T=-78°C; 0.5 h; Inert atmosphere; 2: With oxygen in tetrahydrofuran; toluene T=-78°C; 3: With hydrogenchloride in water T=20°C; pH=1.2;
参考文献
Bonaparte, Amy C.; Betush, Matthew P.; Panseri, Bettina M.; Mastarone, Daniel J.; Murphy, Ryan K.; Murphree, S. Shaun
Organic Letters, 2011 , vol. 13, # 6 p. 1447 - 1449
1: 6-heptenyl bromide With iodine; magnesium in diethyl ether T=34°C; 3.5 h; 2: carbon dioxide in diethyl ether T=-20°C; 2 h; 3: With hydrogenchloride in diethyl ether; water
参考文献
West, Ryan; Panagabko, Candace; Atkinson, Jeffrey
Journal of Organic Chemistry, 2010 , vol. 75, # 9 p. 2883 - 2892
