反应条件
oxalyl dichloride 1.) DMF, MeCN, -18 deg C, 15 min, 2.) MeCN, -18 deg C to 0 deg C, 15 min, 3.) pyridine, MeCN, 0 deg C, 1 h; room temperature, 3.5 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Henschke, Julian P.; Rickards, Rodney W.
Journal of Labelled Compounds and Radiopharmaceuticals, 1998 , vol. 41, # 3 p. 211 - 220