双环[2.2.1]庚烷-1-羧酸合成路线 （共 28 条）
反应条件
tri-n-butyl-tin hydride
参考文献
Neuman, Robert C.; Berge, Charles T.; Binegar, Glen Al.; Adam, Waldemar; Nishizawa, Yoshinori
Journal of Organic Chemistry, 1990 , vol. 55, # 15 p. 4564 - 4568
反应条件
sodium hydroxide Yield given;
参考文献
Adcock, William; Clark, Christopher I.
Journal of Organic Chemistry, 1995 , vol. 60, # 3 p. 723 - 724
参考文献
Kostova; Dimitrov
Synthetic Communications, 1995 , vol. 25, # 10 p. 1575 - 1587
参考文献
Boehme
Journal of the American Chemical Society, 1959 , vol. 81, p. 2762,2764
反应条件
lithium 1.) cyclohexane, reflux, 12 h, 2.) cyclohexane, 5 h; Yield given. Multistep reaction;
参考文献
Greer, Melinda L.; Sarker, Haripada; Mendicino, Maria E.; Blackstock, Silas C.
Journal of the American Chemical Society, 1995 , vol. 117, # 42 p. 10460 - 10467
反应条件
1: n-Bu3SnH, AIBN / diethyl ether / 4 h / 0 °C / Irradiation 2: KOH / aq. ethanol View Scheme
参考文献
Adcock, William; Clark, Christopher I.
Journal of Organic Chemistry, 1995 , vol. 60, # 3 p. 723 - 724
反应条件
in benzene T=81°C; Title compound not separated from byproducts;
参考文献
Fossey, Jacques; Lefort, Daniel
Tetrahedron, 1980 , vol. 36, # 81 p. 1023 - 1036
反应条件
4-(N,N-dimethlyamino)pyridine; Fonderma; 2-methylpropane-2-thiol in benzene HeatingIrradiation;
参考文献
Della, Ernest W.; Tsanaktsidis, John
Australian Journal of Chemistry, 1986 , vol. 39, p. 2061 - 2066
反应条件
1: 1 h / Heating 2: 1) NaBH4, Sn(CH3)3Cl / 1) EtOH, below 15 deg C, irradiation, 3 h, 2) MeCOMe, 15 min 3: 25percent aq. NaOH View Scheme
参考文献
Gudipati, Murthy S.; Radziszewski, Juliusz G.; Kaszynski, Piotr; Michl, Josef
Journal of Organic Chemistry, 1993 , vol. 58, # 14 p. 3668 - 3674
反应条件
1: SOCl2 / 2 h / Heating 2: 1 h / Heating 3: 1) NaBH4, Sn(CH3)3Cl / 1) EtOH, below 15 deg C, irradiation, 3 h, 2) MeCOMe, 15 min 4: 25percent aq. NaOH View Scheme
参考文献
Gudipati, Murthy S.; Radziszewski, Juliusz G.; Kaszynski, Piotr; Michl, Josef
Journal of Organic Chemistry, 1993 , vol. 58, # 14 p. 3668 - 3674
