2-氯-3-硝基-6-苯基吡啶合成路线 （共 4 条）
反应条件
caesium carbonate; tetrakis(triphenylphosphine) palladium(0) in 1,4-dioxane; water T=100°C; 0.166667 h; Microwave irradiation;
参考文献
Smithkline Beecham Corporation
Patent: US2008/242685 A1, 2008 ;
Location in patent: Page/Page column 16 ;
反应条件
hydrogenchloride; sodium nitrite Ambient temperature;
参考文献
Troschuetz, Reinhard; Karger, Alexander
Journal of Heterocyclic Chemistry, 1997 , vol. 34, # 4 p. 1147 - 1151
反应条件
potassium phosphate; dichloro(cycloocta-1,5-diene)palladium(II); 1-Mes2B-2-Ph2P-(C6H4) in toluene T=100°C; Suzuki-Miyaura Coupling; 5 h; Schlenk techniqueGloveboxInert atmosphere; Reagent/catalystTime; regioselective reaction;
参考文献
Malacea, Raluca; Chahdoura, Faouzi; Devillard, Marc; Saffon, Nathalie; Gomez, Montserrat; Bourissou, Didier
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 11-12 p. 2274 - 2284
反应条件
1: AcOH / ethanol / Heating 2: 45 percent / aq. HCl, NaNO2 / Ambient temperature View Scheme
参考文献
Troschutz; Karger
Journal of Heterocyclic Chemistry, 1996 , vol. 33, # 6 p. 1815 - 1821
