2,3,4,6-四-O-(2,2-二甲基丙烷酰基)-D-甘露糖基氟化物合成路线 （共 3 条）
反应条件
4-(N,N-dimethlyamino)pyridine in pyridine T=0 - 70°C; Acylation;
参考文献
Scott, Ian L.; Market, Robert V.; DeOrazio, Russell J.; Meckler, Harold; Kogan, Timothy P.
Carbohydrate Research, 1999 , vol. 317, # 1-4 p. 210 - 216
反应条件
1: 83 percent / HF; pyridine / CH2Cl2 / 40 °C / sealed PFE flask 2: K2CO3 / methanol / 20 °C 3: 80 percent / 4-dimethylaminopyridine / pyridine / 0 - 70 °C View Scheme
参考文献
Scott, Ian L.; Market, Robert V.; DeOrazio, Russell J.; Meckler, Harold; Kogan, Timothy P.
Carbohydrate Research, 1999 , vol. 317, # 1-4 p. 210 - 216
反应条件
1: K2CO3 / methanol / 20 °C 2: 80 percent / 4-dimethylaminopyridine / pyridine / 0 - 70 °C View Scheme
参考文献
Scott, Ian L.; Market, Robert V.; DeOrazio, Russell J.; Meckler, Harold; Kogan, Timothy P.
Carbohydrate Research, 1999 , vol. 317, # 1-4 p. 210 - 216
