2,6-二甲基-3H-喹唑啉-4-酮合成路线 （共 13 条）
反应条件
ammonium hydroxide in ethanol T=20°C; 48 h;
参考文献
Cao, Sheng-Li; Feng, Yu-Ping; Zheng, Xiao-Lin; Jiang, Yu-Yang; Zhang, Mei; Wang, Yue; Xu, Meng
Archiv der Pharmazie, 2006 , vol. 339, # 5 p. 250 - 254
反应条件
1: in N,N-dimethyl-formamide T=20°C; 0.166667 h; Inert atmosphere; 2: With anhydrous iron chloride; caesium carbonate; L-proline in N,N-dimethyl-formamide Microwave irradiationInert atmosphere;
参考文献
Zhang, Xiaodong; Ye, Deju; Sun, Haifeng; Guo, Diliang; Wang, Jiang; Huang, He; Zhang, Xu; Jiang, Hualiang; Liu, Hong
Green Chemistry, 2009 , vol. 11, # 11 p. 1881 - 1888
反应条件
palladium 10 on activated carbon; ammonium formate; acetic acid T=20 - 80°C; Inert atmosphere;
参考文献
Gupta, Sahaj; Agarwal, Piyush K.; Kundu, Bijoy
Tetrahedron Letters, 2010 , vol. 51, # 14 p. 1887 - 1890
反应条件
1: T=120°C; 3 h; 2: With ammonia in water 4 h; Reflux;
参考文献
Okano, Masahiko; Mito, Jun; Maruyama, Yasufumi; Masuda, Hirofumi; Niwa, Tomoko; Nakagawa, Shin-ichiro; Nakamura, Yoshitaka; Matsuura, Akira
Bioorganic and Medicinal Chemistry, 2009 , vol. 17, # 1 p. 119 - 132
反应条件
1: N-(2,4-dimethylphenyl)acetamide With potassium permanganate in water T=80°C; 2: acetic anhydride in Petroleum ether 3 h; Heating; 3: With ammonium acetate; acetic acid in Petroleum ether Heating;
参考文献
Chen, Shiyan; Lin, Jimao; Qin, Bingjie
Organic Preparations and Procedures International, 2004 , vol. 36, # 3 p. 277 - 279
参考文献
Cao, Sheng-Li; Feng, Yu-Ping; Jiang, Yu-Yang; Liu, Shi-Ying; Ding, Guo-Yu; Li, Run-Tao
Bioorganic and Medicinal Chemistry Letters, 2005 , vol. 15, # 7 p. 1915 - 1917
反应条件
1: 92 percent / 1.5 h / Heating 2: 89 percent / aq. NH3 / ethanol / 48 h / 20 °C View Scheme
参考文献
Patil; Jones; Nair; Galivan; Maley; Kisliuk; Gaumont; Duch; Ferone
Journal of Medicinal Chemistry, 1989 , vol. 32, # 6 p. 1284 - 1289
反应条件
phosphorus pentoxide; xylene T=145 - 150°C;
参考文献
Bhattacharyya; Bose; Ray
Journal of the Indian Chemical Society, 1929 , vol. 6, p. 282
Chem. Zentralbl., 1929 , vol. 100, # II p. 887
反应条件
chromium(VI) oxide; acetic acid
参考文献
Bischler; Muntendam
Chemische Berichte, 1895 , vol. 28, p. 729
反应条件
Yield given. Multistep reaction;
参考文献
Patil; Jones; Nair; Galivan; Maley; Kisliuk; Gaumont; Duch; Ferone
Journal of Medicinal Chemistry, 1989 , vol. 32, # 6 p. 1284 - 1289
