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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
18732-50-8
合成路线
（共 12 条）
644-78-0
2-羟基查耳酮
→
反应条件
18732-50-8
反应条件
hydroxylamine hydrochloride; potassium hydroxide in methanol 12 h; Reflux;
参考文献
Mokale, Santosh N.; Nevase, Manjusha C.; Sakle, Nikhil S.; Dube, Pritam N.; Shelke, Vishakha R.; Bhavale, Swati A.; Begum, Afreen
Bioorganic and Medicinal Chemistry Letters, 2014 , vol. 24, # 9 p. 2155 - 2158
837383-20-7
→
反应条件
18732-50-8
反应条件
iodine; sodium hydrogencarbonate; potassium iodide in tetrahydrofuran; water 4.5 h; Heating;
参考文献
Basinski, W.
Polish Journal of Chemistry, 1995 , vol. 69, # 4 p. 579 - 582
94-67-7
水杨醛肟
+
536-74-3
苯乙炔
→
反应条件
18732-50-8
反应条件
pyridine; N-chloro-succinimide in chloroform 2 h; Heating;
参考文献
Thomsen, Ib; Torssell, Kurt B. G.
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1988 , vol. 42, # 5 p. 303 - 308
119841-74-6
+
7196-01-2
→
反应条件
18732-50-8
反应条件
triethylamine in chloroform 0.5 h; Heating;
参考文献
Thomsen, Ib; Torssell, Kurt B. G.
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1988 , vol. 42, # 5 p. 303 - 308
39729-11-8
→
反应条件
18732-50-8
反应条件
potassium hydroxide; hydroxylamine hydrochloride in ethanol Heating;
参考文献
Murthy; Rao
Journal of the Indian Chemical Society, 1973 , vol. 50, # 3 p. 213 - 214
4010-33-7
2-乙酰苯基苯甲酸酯
→
反应条件
18732-50-8
反应条件
1: pyridine, KOH (molten) / 1.) 2 h; 2.) overnight 2: 420 percent / hydroxylamine hydrochloride / dimethylformamide; H2O / 4 h / Heating View Scheme
参考文献
Naphade, V. J.; Ghiya, B. J.
Journal of the Indian Chemical Society, 1986 , vol. 63, p. 851 - 853
118-93-4
2'-羟基苯乙酮
→
反应条件
18732-50-8
反应条件
1: pyridine, phosphorous oxychloride / 3 h / 50 °C 2: pyridine, KOH (molten) / 1.) 2 h; 2.) overnight 3: 420 percent / hydroxylamine hydrochloride / dimethylformamide; H2O / 4 h / Heating View Scheme
参考文献
Naphade, V. J.; Ghiya, B. J.
Journal of the Indian Chemical Society, 1986 , vol. 63, p. 851 - 853
98-88-4
苯甲酰氯
→
反应条件
18732-50-8
反应条件
1: pyridine, phosphorous oxychloride / 3 h / 50 °C 2: pyridine, KOH (molten) / 1.) 2 h; 2.) overnight 3: 420 percent / hydroxylamine hydrochloride / dimethylformamide; H2O / 4 h / Heating View Scheme
参考文献
Naphade, V. J.; Ghiya, B. J.
Journal of the Indian Chemical Society, 1986 , vol. 63, p. 851 - 853
90-02-8
水杨醛
→
反应条件
18732-50-8
反应条件
1: sodium hydroxide / ethanol; water / 2 h 2: hydroxylamine hydrochloride; potassium hydroxide / methanol / 12 h / |Reflux View Scheme
参考文献
Mokale, Santosh N.; Nevase, Manjusha C.; Sakle, Nikhil S.; Dube, Pritam N.; Shelke, Vishakha R.; Bhavale, Swati A.; Begum, Afreen
Bioorganic and Medicinal Chemistry Letters, 2014 , vol. 24, # 9 p. 2155 - 2158
98-86-2
苯乙酮
→
反应条件
18732-50-8
反应条件
1: sodium hydroxide / ethanol; water / 2 h 2: hydroxylamine hydrochloride; potassium hydroxide / methanol / 12 h / |Reflux View Scheme
参考文献
Mokale, Santosh N.; Nevase, Manjusha C.; Sakle, Nikhil S.; Dube, Pritam N.; Shelke, Vishakha R.; Bhavale, Swati A.; Begum, Afreen
Bioorganic and Medicinal Chemistry Letters, 2014 , vol. 24, # 9 p. 2155 - 2158
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