2-(吡啶-2-基氨基)乙基氨基甲酸叔丁酯合成路线 (共 4 条)
反应条件
cyclohexene; palladium on activated charcoal in isopropyl alcohol Heating;
参考文献
Keenan, Richard M.; Miller, William H.; Barton, Linda S.; Bondinell, William E.; Cousins, Russell D.; Eppley, Daniel F.; Hwang, Shing-Mei; Kwon, Chet; Lago, M. Amparo; Nguyen, Thomas T.; Smith, Brian R.; Uzinskas, Irene N.; Yuan, Catherine C. K.
Bioorganic and Medicinal Chemistry Letters, 1999 , vol. 9, # 13 p. 1801 - 1806
反应条件
palladium monocarbide in ethanol; cyclohexene
参考文献
SmithKline Beecham Corporation
Patent: US6069158 A1, 2000 ;
反应条件
1: 89 percent / NaHCO3 / 2-methyl-butan-2-ol / Heating 2: 78 percent / cyclohexene / 10 percent Pd/C / propan-2-ol / Heating View Scheme
参考文献
Keenan, Richard M.; Miller, William H.; Barton, Linda S.; Bondinell, William E.; Cousins, Russell D.; Eppley, Daniel F.; Hwang, Shing-Mei; Kwon, Chet; Lago, M. Amparo; Nguyen, Thomas T.; Smith, Brian R.; Uzinskas, Irene N.; Yuan, Catherine C. K.
Bioorganic and Medicinal Chemistry Letters, 1999 , vol. 9, # 13 p. 1801 - 1806
反应条件
hydrogenchloride in 1,4-dioxane; dichloromethane
T=0 - 20°C;
参考文献
Keenan, Richard M.; Miller, William H.; Barton, Linda S.; Bondinell, William E.; Cousins, Russell D.; Eppley, Daniel F.; Hwang, Shing-Mei; Kwon, Chet; Lago, M. Amparo; Nguyen, Thomas T.; Smith, Brian R.; Uzinskas, Irene N.; Yuan, Catherine C. K.
Bioorganic and Medicinal Chemistry Letters, 1999 , vol. 9, # 13 p. 1801 - 1806