5,11-二氢-6H-吲哚并[3,2-c]喹啉-6-酮合成路线 (共 35 条)
反应条件
copper(l) iodide in acetonitrile T=20°C; 1 h; Photolysis;
参考文献
Shi, Zongjun; Ren, Yuwei; Li, Bing; Lu, Shenci; Zhang, Wei
Chemical Communications, 2010 , vol. 46, # 22 p. 3973 - 3975
反应条件
1: in diphenylether T=250°C; Fischer indolization; 0.5 h; 2: With palladium on activated charcoal in diphenylether T=250°C; 3 h;
参考文献
Chen, Yeh-Long; Chung, Chao-Ho; Chen, I-Li; Chen, Po-Hsu; Jeng, Haw-Yaun
Bioorganic and medicinal chemistry, 2002 , vol. 10, # 8 p. 2705 - 2712
反应条件
in 1,2-dichloro-benzene T=180°C; 0.25 h; Inert atmosphere;
参考文献
Hayashi, Kaori; Choshi, Tominari; Chikaraishi, Kyoko; Oda, Aimi; Yoshinaga, Rikako; Hatae, Noriyuki; Ishikura, Minoru; Hibino, Satoshi
Tetrahedron, 2012 , vol. 68, # 22 p. 4274 - 4279
反应条件
acetic acid 2 h; Heating;
参考文献
Bergman, Jan; Engqvist, Robert; Stalhandske, Claes; Wallberg, Hans
Tetrahedron, 2003 , vol. 59, # 7 p. 1033 - 1048
反应条件
sodium hydride in N,N-dimethyl-formamide; mineral oil T=120°C; 1 h;
参考文献
Zhang, Xiang; Zhang-Negrerie, Daisy; Deng, Jun; Du, Yunfei; Zhao, Kang
Journal of Organic Chemistry, 2013 , vol. 78, # 24 p. 12750 - 12759
反应条件
dichloro bis(acetonitrile) palladium(II); cupric trifluoroacetate; trifluoroacetic acid in 1,4-dioxane T=110°C;
参考文献
Liang, Dongdong; Hu, Ziwei; Peng, Jiangling; Huang, Jinbo; Zhu, Qiang
Chemical Communications, 2013 , vol. 49, # 2 p. 173 - 175
反应条件
in toluene T=100°C; 12 h;
参考文献
Molina, Pedro; Alajarin, Mateo; Vidal, Angel
Tetrahedron Letters, 1989 , vol. 30, # 21 p. 2847 - 2850
反应条件
oxygen; palladium on activated charcoal in diphenylether 48 h; Heating;
参考文献
Stadlbauer, Wolfgang; Kappe, Thomas
Monatshefte fuer Chemie, 1984 , vol. 115, p. 467 - 476
反应条件
acetic acid 2 h; Heating;
参考文献
Bergman, Jan; Engqvist, Robert; Stalhandske, Claes; Wallberg, Hans
Tetrahedron, 2003 , vol. 59, # 7 p. 1033 - 1048
反应条件
1: 34 percent / aq. HCl / methanol / 25 h / 20 °C 2: 70 percent / AcOH / 1 h / Heating View Scheme
参考文献
Tetrahedron, , vol. 59, # 7 p. 1033 - 1048