2-(2-甲氧基苯基)-5-苯基-1,3,4-恶二唑合成路线 （共 11 条）
反应条件
2,4,6-tris[(4-dichloroiodo)phenoxy]-1,3,5-triazine in dichloromethane T=20°C;
参考文献
Thorat, Prerana B.; Bhong, Bhagyashree Y.; Karade, Nandkishor Y.
Synlett, 2013 , vol. 24, # 16 art. no. ST-2013-D0533-L, p. 2061 - 2066
反应条件
pyridine; thionyl chloride T=80°C; 4 h;
参考文献
Tanaka, Hiromitsu; Tokito, Shizuo; Taga, Yasunori; Okada, Akane
Journal of Materials Chemistry, 1998 , vol. 8, # 9 p. 1999 - 2003
反应条件
1: With N-ethyl-N,N-diisopropylamine; HATU in tetrahydrofuran T=20°C; 0.75 h; 2: With Burgess Reagent in tetrahydrofuran T=20°C;
参考文献
Li, Changkun; Dickson, Hamilton D.
Tetrahedron Letters, 2009 , vol. 50, # 47 p. 6435 - 6439
反应条件
lead dioxide in acetic acid T=90 - 100°C; 0.5 h;
参考文献
Milcent, Rene; Barbier, Geo
Journal of Heterocyclic Chemistry, 1983 , vol. 20, p. 77 - 80
反应条件
trichlorophosphate 0.2 h; microwave irradiation;
参考文献
Khan, Mahmud Tareq Hassan; Choudhary, Muhammad Iqbal; Khan, Khalid Mohammed; Rani, Mubeen; Atta-ur-Rahman
Bioorganic and Medicinal Chemistry, 2005 , vol. 13, # 10 p. 3385 - 3395
反应条件
1: 71 percent / Na2CO3 / dioxane / 2 h / 20 - 90 °C 2: 100 percent / thionyl chloride, pyridine / 4 h / 80 °C View Scheme
参考文献
Tanaka, Hiromitsu; Tokito, Shizuo; Taga, Yasunori; Okada, Akane
Journal of Materials Chemistry, 1998 , vol. 8, # 9 p. 1999 - 2003
反应条件
1: 71 percent / Na2CO3 / dioxane / 2 h / 20 - 90 °C 2: 100 percent / thionyl chloride, pyridine / 4 h / 80 °C View Scheme
参考文献
Tanaka, Hiromitsu; Tokito, Shizuo; Taga, Yasunori; Okada, Akane
Journal of Materials Chemistry, 1998 , vol. 8, # 9 p. 1999 - 2003
反应条件
1: triethylamine / chloroform / 2 h / 20 °C 2: trichlorophosphate / 5 h / |Inert atmosphere; |Reflux View Scheme
参考文献
Li, Hong-Yan; Li, Tian-Yi; Teng, Ming-Yu; Xu, Qiu-Lei; Zhang, Song; Jin, Yi-Ming; Liu, Xuan; Zheng, You-Xuan; Zuo, Jing-Lin
Journal of Materials Chemistry C, 2014 , vol. 2, # 6 p. 1116 - 1124
反应条件
1: triethylamine / chloroform / 2 h / 20 °C 2: trichlorophosphate / 5 h / |Inert atmosphere; |Reflux View Scheme
参考文献
Li, Hong-Yan; Li, Tian-Yi; Teng, Ming-Yu; Xu, Qiu-Lei; Zhang, Song; Jin, Yi-Ming; Liu, Xuan; Zheng, You-Xuan; Zuo, Jing-Lin
Journal of Materials Chemistry C, 2014 , vol. 2, # 6 p. 1116 - 1124
参考文献
Russo; Ghelardoni
Bollettino chimico farmaceutico, 1966 , vol. 105, # 12 p. 911 - 921
