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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
18740-66-4
合成路线
（共 8 条）
529-33-9
1,2,3,4-四氢-1-萘酚
+
18740-66-4
→
反应条件
53732-47-1
(S)-(+)-1,2,3,4-四氢-1-萘酚
反应条件
1: 1-hydroxy-1,2,3,4-tetrahydronaphthalene With (-)-Tetramisole; N-ethyl-N,N-diisopropylamine in tetrahydrofuran T=-78°C; Inert atmosphereMolecular sieveResolution of racemate; 2: chlorotris(p-methylphenyl)silane in tetrahydrofuran T=-78°C; 48 h; Inert atmosphereMolecular sieveResolution of racemate; enantioselective reaction;
参考文献
Akhani, Ravish K.; Moore, Maggie I.; Pribyl, Julia G.; Wiskur, Sheryl L.
Journal of Organic Chemistry, 2014 , vol. 79, # 6 p. 2384 - 2396
1481-93-2
4-色原烷醇
+
18740-66-4
→
反应条件
53732-47-1
(S)-(+)-1,2,3,4-四氢-1-萘酚
反应条件
1: cis-4-hydroxy-3,4-dihydro-1-benzopyran With (-)-Tetramisole; N-ethyl-N,N-diisopropylamine in tetrahydrofuran T=-78°C; Inert atmosphereMolecular sieveResolution of racemate; 2: chlorotris(p-methylphenyl)silane in tetrahydrofuran T=-78°C; 48 h; Inert atmosphereMolecular sieveResolution of racemate; enantioselective reaction;
参考文献
Akhani, Ravish K.; Moore, Maggie I.; Pribyl, Julia G.; Wiskur, Sheryl L.
Journal of Organic Chemistry, 2014 , vol. 79, # 6 p. 2384 - 2396
18740-66-4
+
141-52-6
乙醇钠
→
反应条件
18742-54-6
反应条件
暂无反应条件数据
参考文献
Brook; Mauris
Journal of the American Chemical Society, 1957 , vol. 79, p. 971
529-33-9
1,2,3,4-四氢-1-萘酚
+
18740-66-4
→
反应条件
53732-47-1
(S)-(+)-1,2,3,4-四氢-1-萘酚
反应条件
1: 1-hydroxy-1,2,3,4-tetrahydronaphthalene With (-)-Tetramisole; N-ethyl-N,N-diisopropylamine in tetrahydrofuran T=-78°C; Inert atmosphereMolecular sieveResolution of racemate; 2: chlorotris(p-methylphenyl)silane in tetrahydrofuran T=-78°C; 48 h; Inert atmosphereMolecular sieveResolution of racemate; enantioselective reaction;
参考文献
Akhani, Ravish K.; Moore, Maggie I.; Pribyl, Julia G.; Wiskur, Sheryl L.
Journal of Organic Chemistry, 2014 , vol. 79, # 6 p. 2384 - 2396
1481-93-2
4-色原烷醇
+
18740-66-4
→
反应条件
53732-47-1
(S)-(+)-1,2,3,4-四氢-1-萘酚
反应条件
1: cis-4-hydroxy-3,4-dihydro-1-benzopyran With (-)-Tetramisole; N-ethyl-N,N-diisopropylamine in tetrahydrofuran T=-78°C; Inert atmosphereMolecular sieveResolution of racemate; 2: chlorotris(p-methylphenyl)silane in tetrahydrofuran T=-78°C; 48 h; Inert atmosphereMolecular sieveResolution of racemate; enantioselective reaction;
参考文献
Akhani, Ravish K.; Moore, Maggie I.; Pribyl, Julia G.; Wiskur, Sheryl L.
Journal of Organic Chemistry, 2014 , vol. 79, # 6 p. 2384 - 2396
18740-66-4
→
反应条件
15931-53-0
六(4-甲基苯基)二硅烷
反应条件
sodium; xylene
参考文献
Brook; Gilman
Journal of the American Chemical Society, 1954 , vol. 76, p. 2338,2339
Full Text Show Details
Brook; Mauris
Journal of the American Chemical Society, 1957 , vol. 79, p. 971
18740-66-4
→
反应条件
4569-24-8
反应条件
ammonia; acetone
参考文献
Gmelin Handbook: Si: MVol.C, 89, page 242 - 246
18740-66-4
→
反应条件
4620-79-5
三(4-甲基苯基)硅
反应条件
lithium aluminium tetrahydride
参考文献
Brook; Gilman
Journal of the American Chemical Society, 1954 , vol. 76, p. 2338,2339
