3,4,5-三甲氧基肉桂酸乙酯合成路线 (共 24 条)
反应条件
in dichloromethane T=20°C; Wittig olefination; 5 h;
参考文献
European Journal of Organic Chemistry, , # 26 p. 5100 - 5107
反应条件
potassium carbonate in water T=70°C; 4 h;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 37, # 1 p. 68 - 72
反应条件
tributyl-amine; palladium diacetate in xylene T=120°C; 2 h;
参考文献
Journal of Organometallic Chemistry, , vol. 233, # 2 p. 267 - 274
反应条件
triethylamine in acetonitrile 0.166667 h; microwave irradiation, cooling;
参考文献
Helvetica Chimica Acta, , vol. 88, # 4 p. 811 - 816
反应条件
sulfuric acid 24 h; Reflux;
参考文献
Chemical Biology and Drug Design, , vol. 81, # 3 p. 389 - 398
反应条件
1: thionyl chloride, DMF / toluene / 60 - 70 °C 2: 44 percent / tri-n-butylamine, palladium acetate / xylene / 2 h / 120 °C View Scheme
参考文献
Journal of Organometallic Chemistry, , vol. 233, # 2 p. 267 - 274
反应条件
1: piperidine / pyridine 2: H2SO4 View Scheme
参考文献
Canadian Journal of Chemistry, , vol. 48, p. 3882 - 3888
反应条件
piperidine; sulfuric acid 1) pyridine; Yield given. Multistep reaction;
参考文献
European Journal of Medicinal Chemistry, , vol. 23, # 1 p. 53 - 62
参考文献
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, , vol. 35, # 6 p. 419 - 428
反应条件
water; lithium hydroxide hydrate in tetrahydrofuran T=20°C; 12 h;
参考文献
European Journal of Medicinal Chemistry, , vol. 57, p. 344 - 361