反应条件
1.1: 62 percent / imidazole / dimethylformamide / 1 h / 25 °C
2.1: 54 percent / 2,6-lutidine / CH2Cl2 / 3 h / -20 °C
3.1: PCl3; pyridine / 0.25 h / 25 °C
3.2: 1 h
4.1: 3.9 mg / aq. H2O2 / CH2Cl2; pyridine / 0.5 h
5.1: aq. HF / acetonitrile / 0.25 h / 25 °C
5.2: aq. HF; pyridine / acetonitrile / 168000 h
View Scheme
参考文献
Boger; Ichikawa; Zhong
Journal of the American Chemical Society, 2001 , vol. 123, # 18 p. 4161 - 4167
