1-羟基-2,2,5,5-四甲基-4-苯基-3-咪唑啉-3-氧化物合成路线 (共 9 条)
反应条件
hydrogenchloride; sodium nitrite in chloroform; water 0.5 h;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 32, # 2 p. 352 - 355
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 2 p. 391 - 394
反应条件
hydrazine hydrate in ethanol
T=20°C; 1 h;
参考文献
Grigor'ev, I. A.; Shchukin, G. I.; Volodarskii, L. B.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1983 , vol. 32, # 5 p. 1030 - 1035
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1983 , # 5 p. 1140 - 1146
反应条件
bis-triphenylphosphine-palladium(II) chloride; triethylamine in benzene
T=80°C; 4 h;
参考文献
Vasilevsky, Sergei F.; Krivenko, Olga L.; Gorelik, Vitalii R.; Alabugin, Igor V.
Tetrahedron, 2008 , vol. 64, # 37 p. 8807 - 8814
反应条件
ammonium acetate in methanol
4 h; Heating;
参考文献
Reznikov; Volodarsky
Russian Chemical Bulletin, 1997 , vol. 46, # 9 p. 1577 - 1581
反应条件
ammonium acetate in methanol
2 h; Heating;
参考文献
Reznikov; Volodarsky
Russian Chemical Bulletin, 1997 , vol. 46, # 9 p. 1577 - 1581
反应条件
triethylamine in methanol
0.5 h;
参考文献
Shchukin, G. I.; Grigor'ev, I. A.; Volodarskii, L. B.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1983 , vol. 32, # 10 p. 2123 - 2127
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1983 , # 10 p. 2357 - 2360
反应条件
sodium hydroxide; C8H13Cl2N2O2 in ethanol
Further byproducts given. Yields of byproduct given;
参考文献
Grigor'ev, I. A.; Shchukin, G. I.; Volodarskii, L. B.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1983 , vol. 32, # 12 p. 2501 - 2509
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1983 , # 12 p. 2787 - 2797
反应条件
in hexane
T=20°C; Rate constant;
参考文献
Malievskii, A. D.; Koroteev, S. V.; Volodarskii, L. B.; Shapiro, A. B.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1990 , vol. 39, # 11 p. 2331 - 2338
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1990 , # 11 p. 2575 - 2582
反应条件
sodium hydroxide in ethanol
Product distribution;
参考文献
Grigor'ev, I. A.; Shchukin, G. I.; Volodarskii, L. B.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1983 , vol. 32, # 12 p. 2501 - 2509
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1983 , # 12 p. 2787 - 2797