2,2,4,5,5-五甲基-3-咪唑啉-3-氧化物-1-氧基合成路线 (共 8 条)
反应条件
decanesulfonic peracid in acetonitrile T=19.9°C;
参考文献
Safiullin, R. L.; Enikeeva, L. R.; Bukin, I. I.; Mukhametova, G. A.; Shishlov, N. M.; et al.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1990 , vol. 39, # 5.2 p. 1045 - 1047
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1990 , # 5 p. 1162 - 1165
反应条件
decanesulfonic peracid in chloroform Kinetics;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 39, # 6 p. 1136 - 1138
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 6 p. 1265 - 1268
反应条件
hydrazine hydrate in ethanol T=20°C; 1 h;
参考文献
Grigor'ev, I. A.; Shchukin, G. I.; Volodarskii, L. B.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1983 , vol. 32, # 5 p. 1030 - 1035
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1983 , # 5 p. 1140 - 1146
反应条件
triethylamine in methanol 0.5 h;
参考文献
Shchukin, G. I.; Grigor'ev, I. A.; Volodarskii, L. B.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1983 , vol. 32, # 10 p. 2123 - 2127
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1983 , # 10 p. 2357 - 2360
反应条件
in chloroform T=19.9°C; ΔG; Equilibrium constantThermodynamic data;
参考文献
Dikanov, S. A.; Grigor'ev, I. A.; Volodarskii, L. B.; Tsvetkov, Yu. D.
Russian Journal of Physical Chemistry, 1982 , vol. 56, # 11 p. 1696 - 1699
Zhurnal Fizicheskoi Khimii, 1982 , vol. 56, # 11 p. 2762 - 2767
反应条件
potassium hydroxide; bromine; trifluoroacetic acid 1.) methanol, 30 min, 2.) water, pH 7; Yield given. Multistep reaction;
参考文献
Martin, V. V.; Volodarskii, L. B.; Shchukin, G. I.; Vishnivetskaya, L. A.; Grigor'ev, I. A.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1985 , vol. 34, # 1 p. 151 - 158
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1985 , # 1 p. 161 - 169
反应条件
hydrazine hydrate in ethanol
T=20°C; 1 h;
参考文献
Grigor'ev, I. A.; Shchukin, G. I.; Volodarskii, L. B.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1983 , vol. 32, # 5 p. 1030 - 1035
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1983 , # 5 p. 1140 - 1146
反应条件
1: 9 percent / N2H4*H2O / ethanol / 1 h / 20 °C
View Scheme
参考文献
Grigor'ev, I. A.; Shchukin, G. I.; Volodarskii, L. B.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1983 , vol. 32, # 5 p. 1030 - 1035
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1983 , # 5 p. 1140 - 1146