反应条件
1.1: N,N,N',N'-tetramethylethylenediamine; BuLi / diethyl ether; hexane / 20 °C
1.2: 90 percent / 1,2-dibromo-1,1,2,2-tetrafluoroethane / diethyl ether; hexane; tetrahydrofuran / -78 - 20 °C
2.1: NiCl2(dppe) / diethyl ether / Heating
3.1: BBr3 / CH2Cl2 / 0 °C
View Scheme
参考文献
Ooi, Takashi; Takahashi, Makoto; Yamada, Masao; Tayama, Eiji; Omoto, Kiyoyuki; Maruoka, Keiji
Journal of the American Chemical Society, 2004 , vol. 126, # 4 p. 1150 - 1160
