2-(乙酰氨基)-2-脱氧-4-O-(beta-D-吡喃半乳糖基)-beta-D-吡喃葡萄糖基叠氮化物合成路线 (共 4 条)
反应条件
2,6-dimethylpyridine; sodium azide; DMEG in water-d2 T=20°C; 36 h; stereoselective reaction;
参考文献
Tanaka, Tomonari; Nagai, Hikaru; Noguchi, Masato; Kobayashi, Atsushi; Shoda, Shin-Ichiro
Chemical Communications, 2009 , # 23 p. 3378 - 3379
反应条件
1: sodium azide / acetone / 16 h / |Reflux 2: sodium methylate; methanol / 2 h / 0 °C 3: human His6-propeptide-placental catβ1,4-galactosyltransferase 1 fusion protein; Campylobacter jejuni UDP-Glc/GlcNAc-4'-epimerase; alkaline phosphatase / |Enzymatic reaction View Scheme
参考文献
Adamiak, Kathrin; Anders, Thorsten; Henze, Manja; Keul, Helmut; Moeller, Martin; Elling, Lothar
Journal of Molecular Catalysis B: Enzymatic, 2012 , vol. 84, p. 108 - 114
反应条件
1: sodium methylate; methanol / 2 h / 0 °C 2: human His6-propeptide-placental catβ1,4-galactosyltransferase 1 fusion protein; Campylobacter jejuni UDP-Glc/GlcNAc-4'-epimerase; alkaline phosphatase / |Enzymatic reaction View Scheme
参考文献
Adamiak, Kathrin; Anders, Thorsten; Henze, Manja; Keul, Helmut; Moeller, Martin; Elling, Lothar
Journal of Molecular Catalysis B: Enzymatic, 2012 , vol. 84, p. 108 - 114
反应条件
Campylobacter jejuni UDP-Glc/GlcNAc-4'-epimerase; human His6-propeptide-placental catβ1,4-galactosyltransferase 1 fusion protein; alkaline phosphatase Enzymatic reaction;
参考文献
Adamiak, Kathrin; Anders, Thorsten; Henze, Manja; Keul, Helmut; Moeller, Martin; Elling, Lothar
Journal of Molecular Catalysis B: Enzymatic, 2012 , vol. 84, p. 108 - 114