5-甲氧基-2-硝基苯甲酸合成路线 （共 47 条）
反应条件
1: dimethylsulfide borane complex / tetrahydrofuran / 3 h / 80 °C / |Inert atmosphere
2: phosphorus tribromide / diethyl ether / 3 h / |Inert atmosphere
View Scheme
参考文献
Kong, Chen; Jana, Navendu; Driver, Tom G.
Organic Letters, 2013 , vol. 15, # 4 p. 824 - 827
反应条件
borane-THF in tetrahydrofuran
T=0°C; Reflux;
参考文献
BIOGEN IDEC MA INC.; THOMAS, Jermaine; MI, Sha; LIN, Edward, Yin-shiang; ZHENG, Guo, Zhu; MA, Bin; CALDWELL, Richard, D.; GUCKIAN, Kevin; KUMARAVEL, Gnanasambandam
Patent: WO2012/109108 A1, 2012 ;
Location in patent: Page/Page column 39 ;
WO 2012/109108 A1
反应条件
oxygen; silver carbonate; potassium hydroxide; copper(ll) bromide in dimethyl sulfoxide; N,N-dimethyl-formamide
T=130 - 140°C;
参考文献
Luo, Yong; Pan, Xiaolin; Wu, Jie
Tetrahedron Letters, 2010 , vol. 51, # 50 p. 6646 - 6648
反应条件
1: diethyl ether
2: H2 / Raney nickel / methanol
View Scheme
参考文献
Sevbo, D. P.; Stepanova, T. F.; Nekhoroshev, A. A.
Journal of Organic Chemistry USSR (English Translation), 1980 , vol. 16, p. 1097 - 1101
Zhurnal Organicheskoi Khimii, 1980 , vol. 16, # 6 p. 1268 - 1274
反应条件
1: palladium/charcoal; ethanol / Hydrogenation
3: H2O
View Scheme
参考文献
Morrison; Mulholland
Journal of the Chemical Society, 1958 , p. 2702,2703
参考文献
Makino; Takahashi
Journal of the American Chemical Society, 1954 , vol. 76, p. 4994
反应条件
in N,N-dimethyl-formamide
参考文献
American Cyanamid Co.
Patent: US5519133 A1, 1996 ;
