(S,S)-bis(4-benzyl-4,5-dihydrooxazol-4-yl)methylamine; N-ethyl-N,N-diisopropylamine; copper dichloride in dichloromethane
T=0°C; 2 h; Title compound not separated from byproducts;
参考文献
Gissibi, Anja; Finn; Reiser, Oliver
Organic Letters, 2005 , vol. 7, # 12 p. 2325 - 2328
(2S,3R)-3-methyl-2-phenyl-3,4-dihydro-2H-benzo[4,5]thiazolo[3,2-a]pyrimidine; sodium sulfate; N-ethyl-N,N-diisopropylamine in toluene
T=-40°C; 11 h; Resolution of racemate; optical yield given as percent eeenantioselective reaction;
参考文献
Zhang, Yuhua; Birman, Vladimir B.
Advanced Synthesis and Catalysis, 2009 , vol. 351, # 14-15 p. 2525 - 2529
Mueller, Christian E.; Zell, Daniela; Hrdina, Radim; Wende, Raffael C.; Wanka, Lukas; Schuler, Soeren M. M.; Schreiner, Peter R.
Journal of Organic Chemistry, 2013 , vol. 78, # 17 p. 8465 - 8484