1-甲基-3-(1-丙炔基)-苯合成路线 （共 7 条）
反应条件
copper(l) iodide; triethylamine; bis-triphenylphosphine-palladium(II) chloride 24 deg C, then 65 deg C;
参考文献
Pschirer, Neil Gregory; Bunz, Uwe H. F.
Tetrahedron Letters, 1999 , vol. 40, # 13 p. 2481 - 2484
反应条件
1: 46 percent / KOH / ethanol / Heating 2: 1.) Li, Fe(NO3)3 / 1.) liq.NH3, HMPA, 30 min; 2.) 6 h View Scheme
参考文献
Mesnard, Danielle; Bernadou, Francoise; Miginiac, Leone
Journal of Chemical Research, Miniprint, 1981 , # 9 p. 3216 - 3245
反应条件
1: 84 percent / PCl5 / 12 h / 20 °C 2: 46 percent / KOH / ethanol / Heating 3: 1.) Li, Fe(NO3)3 / 1.) liq.NH3, HMPA, 30 min; 2.) 6 h View Scheme
参考文献
Mesnard, Danielle; Bernadou, Francoise; Miginiac, Leone
Journal of Chemical Research, Miniprint, 1981 , # 9 p. 3216 - 3245
反应条件
lithium; iron nitrate (III) 1.) liq.NH3, HMPA, 30 min; 2.) 6 h; Yield given. Multistep reaction;
参考文献
Mesnard, Danielle; Bernadou, Francoise; Miginiac, Leone
Journal of Chemical Research, Miniprint, 1981 , # 9 p. 3216 - 3245
反应条件
(i) PCl5, (ii) NaOiPr; Multistep reaction;
参考文献
Thigpen,A.B.; Fuchs,R.
Journal of Organic Chemistry, 1969 , vol. 34, # 3 p. 505 - 509
反应条件
1: (i) nBuNH2, (ii) Fe, FeCl3*6H2O, aq. HCl 2: (i) PCl5, (ii) NaOiPr View Scheme
参考文献
Thigpen,A.B.; Fuchs,R.
Journal of Organic Chemistry, 1969 , vol. 34, # 3 p. 505 - 509
反应条件
(i), (ii) Na, DMSO; Multistep reaction;
参考文献
Becker,J.Y.
Journal of Organometallic Chemistry, 1976 , vol. 118, p. 247 - 252
