188290-36-0合成路线 （共 917 条）
反应条件
1: thiophene With n-butyllithium in diethyl ether; hexane T=0°C; 1 h; 2: With zinc(II) chloride in diethyl ether; hexane T=0°C; 1 h; 3: 2,3,5-tribromothiophene With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride in diethyl ether; hexane T=20°C; regioselective reaction;
参考文献
Amb, Chad M.; Rasmussen, Seth C.
European Journal of Organic Chemistry, 2008 , # 5 p. 801 - 804
反应条件
aluminium trichloride in nitromethane 1 h, 0-5 degC then room temperature;
参考文献
Jagodzinski, Tadeusz; Jagodzinska, Elzbieta; Jablonski, Zygfryd
Tetrahedron, 1986 , vol. 42, # 13 p. 3683 - 3688
反应条件
tin(IV) chloride; benzene
参考文献
Royer; Demerseman
Bulletin de la Societe Chimique de France, 1959 , p. 1682,1685
参考文献
Gallucci, Judith C.; Mathur, Naresh; Shechter, Harold
Acta Crystallographica, Section C: Crystal Structure Communications, 1995 , vol. 51, # 6 p. 1221 - 1223
反应条件
tin(IV) chloride; benzene
参考文献
Royer; Demerseman
Bulletin de la Societe Chimique de France, 1959 , p. 1682,1685
参考文献
Wynberg; Bantjes
Journal of Organic Chemistry, 1959 , vol. 24, p. 1421
反应条件
in thiophene was heated at 70°C for 2h; was filtered; filtrate was concentrated under reduced pressure; was diluted with hexane; GLC;
参考文献
Fuchita, Yoshio; Hiraki, Katsuma; Kamogawa, Yasuko; Suenaga, Miho; Tohgoh, Kazutaka; Fujiwara, Yuzo
Bulletin of the Chemical Society of Japan, 1989 , vol. 62, # 4 p. 1081 - 1085
反应条件
T=876.84 - 926.84°C; IR laser powering; Product distribution; Further Variations:Reagents;
参考文献
Hore, Nathan R.; Russell, Douglas K.
New Journal of Chemistry, 2004 , vol. 28, # 5 p. 606 - 613
反应条件
T=175°C; 24 h; also 185 deg C and 40 h; Product distribution;
参考文献
Journal of Fluorine Chemistry, , vol. 17, p. 345 - 356
反应条件
in acetonitrile 3 h; Irradiation;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1777 - 1780
