188290-36-0合成路线 （共 917 条）
反应条件
1: With mercury(II) diacetate in acetic acid 15 h; Heating; 2: With iodine in acetic acid 1.5 h; Heating;
参考文献
De, Puran K.; Neckers, Douglas C.
Organic Letters, 2012 , vol. 14, # 1 p. 78 - 81
反应条件
tin(IV) chloride; benzene
参考文献
Fan, Jinmin; Wan, Changfeng; Sun, Gaojun; Wang, Zhiyong
Journal of Organic Chemistry, 2008 , vol. 73, # 21 p. 8608 - 8611
反应条件
1: thiophene With n-butyllithium in tetrahydrofuran; hexane T=-78°C; 0.833333 h; 2: 1-n-heptylbromide in tetrahydrofuran; hexane T=-78 - 20°C;
参考文献
Pu, Shouzhi; Zhu, Shengsheng; Rao, Yi; Liu, Gang; Wei, Huizhen
Journal of Molecular Structure, 2009 , vol. 921, # 1-3 p. 89 - 100
反应条件
1: thiophene With n-butyllithium in hexane T=-78°C; 1 h; 2: 1-iodo-n-heptane in hexane T=-78 - 20°C;
参考文献
Wilson, Paul; Lacey, David; Sharma, Sanjay; Worthington, Brenda
Molecular Crystals and Liquid Crystals Science and Technology Section A: Molecular Crystals and Liquid Crystals, 2001 , vol. 368, p. 279 - 292
反应条件
1: thiophene With n-butyllithium in diethyl ether; hexane T=-71 - 20°C; 2: cyclo-(Me2SiO)3 in diethyl ether; hexane T=-71 - 20°C;
参考文献
Denmark, Scott E.; Baird, John D.; Regens, Christopher S.
Journal of Organic Chemistry, 2008 , vol. 73, # 4 p. 1440 - 1455
反应条件
1: thiophene With potassium permanganate; acetic acid Microwave irradiation; 2: (3-formyl-4-methoxyphenyl)boronic acid 0.5 h; Microwave irradiation;
参考文献
Demir, Ayhan S.; Findik, Hamide; Saygili, Nezire; Tuna Subasi
Tetrahedron, 2010 , vol. 66, # 6 p. 1308 - 1312
反应条件
n-butyllithium; diethyl ether anschliessend Erwaermen mit Chlor-triphenyl-silan;
参考文献
Gilman et al.
Journal of the American Chemical Society, 1950 , vol. 72, p. 1689
反应条件
1: With N,N,N',N,-tetramethylethylenediamine; sec.-butyllithium in hexane T=20 - 60°C; 1 h; 2: With water-d2 in diethyl ether Molecular sieveInert atmosphere;
参考文献
Lin, Sibo; Herbert, David E.; Velian, Alexandra; Day, Michael W.; Agapie, Theodor
Journal of the American Chemical Society, 2013 , vol. 135, # 42 p. 15830 - 15840
反应条件
deuterium; oxide-CMA T=174.9°C; var. CMA cat.,; Rate constantProduct distribution;
参考文献
John, Christopher S.; Williamson, James G.; Kennedy, Lois V. F.; Tyler, J. Kelvin
Journal of the Chemical Society, Faraday Transactions 1: Physical Chemistry in Condensed Phases, 1980 , vol. 76, p. 1356 - 1365
反应条件
palladium diacetate; air; sodium nitrite in acetic acid 7 h; Heating;
参考文献
Itahara; Ebihara; Kawasaki
Bulletin of the Chemical Society of Japan, 1983 , vol. 56, # 7 p. 2171 - 2172
